{"id":"https://openalex.org/W2085127298","doi":"https://doi.org/10.1109/iceee.2013.6676015","title":"Synthesis and characterization of nanoestructured TiO<sub>2</sub> anatase-phase powders obtained by the homogeneous precipitation method","display_name":"Synthesis and characterization of nanoestructured TiO<sub>2</sub> anatase-phase powders obtained by the homogeneous precipitation method","publication_year":2013,"publication_date":"2013-09-01","ids":{"openalex":"https://openalex.org/W2085127298","doi":"https://doi.org/10.1109/iceee.2013.6676015","mag":"2085127298"},"language":"en","primary_location":{"id":"doi:10.1109/iceee.2013.6676015","is_oa":false,"landing_page_url":"https://doi.org/10.1109/iceee.2013.6676015","pdf_url":null,"source":null,"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"2013 10th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)","raw_type":"proceedings-article"},"type":"article","indexed_in":["crossref"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5066236725","display_name":"Jes\u00fas M.N. Morales","orcid":"https://orcid.org/0000-0003-1321-7172"},"institutions":[{"id":"https://openalex.org/I68368234","display_name":"Centro de Investigaci\u00f3n y de Estudios Avanzados del Instituto Polit\u00e9cnico Nacional","ror":"https://ror.org/009eqmr18","country_code":"MX","type":"facility","lineage":["https://openalex.org/I59361560","https://openalex.org/I68368234"]}],"countries":["MX"],"is_corresponding":false,"raw_author_name":"J. Morales","raw_affiliation_strings":["Departamento de Ingenier\u00eda El\u00e9ctrica, CINVESTAV-IPN, SEES, M\u00e9xico, D.F","Dept. de Ing. Electr., Centro de Investig. y de Estudios Av. del Inst., Mexico City, Mexico"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Departamento de Ingenier\u00eda El\u00e9ctrica, CINVESTAV-IPN, SEES, M\u00e9xico, D.F","institution_ids":["https://openalex.org/I68368234"]},{"raw_affiliation_string":"Dept. de Ing. Electr., Centro de Investig. y de Estudios Av. del Inst., Mexico City, Mexico","institution_ids":[]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5037818583","display_name":"A. Maldonado","orcid":"https://orcid.org/0000-0001-8898-3248"},"institutions":[{"id":"https://openalex.org/I68368234","display_name":"Centro de Investigaci\u00f3n y de Estudios Avanzados del Instituto Polit\u00e9cnico Nacional","ror":"https://ror.org/009eqmr18","country_code":"MX","type":"facility","lineage":["https://openalex.org/I59361560","https://openalex.org/I68368234"]}],"countries":["MX"],"is_corresponding":false,"raw_author_name":"A. Maldonado","raw_affiliation_strings":["Departamento de Ingenier\u00eda El\u00e9ctrica, CINVESTAV-IPN, SEES, M\u00e9xico, D.F","Dept. de Ing. Electr., Centro de Investig. y de Estudios Av. del Inst., Mexico City, Mexico"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Departamento de Ingenier\u00eda El\u00e9ctrica, CINVESTAV-IPN, SEES, M\u00e9xico, D.F","institution_ids":["https://openalex.org/I68368234"]},{"raw_affiliation_string":"Dept. de Ing. Electr., Centro de Investig. y de Estudios Av. del Inst., Mexico City, Mexico","institution_ids":[]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5058174441","display_name":"M. de la L. Olvera","orcid":"https://orcid.org/0000-0001-9270-6497"},"institutions":[{"id":"https://openalex.org/I68368234","display_name":"Centro de Investigaci\u00f3n y de Estudios Avanzados del Instituto Polit\u00e9cnico Nacional","ror":"https://ror.org/009eqmr18","country_code":"MX","type":"facility","lineage":["https://openalex.org/I59361560","https://openalex.org/I68368234"]}],"countries":["MX"],"is_corresponding":false,"raw_author_name":"M. de la L. Olvera","raw_affiliation_strings":["Departamento de Ingenier\u00eda El\u00e9ctrica, CINVESTAV-IPN, SEES, Mexico","Dept. de Ing. Electr., Centro de Investig. y de Estudios Av. del Inst., Mexico City, Mexico"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Departamento de Ingenier\u00eda El\u00e9ctrica, CINVESTAV-IPN, SEES, Mexico","institution_ids":["https://openalex.org/I68368234"]},{"raw_affiliation_string":"Dept. de Ing. Electr., Centro de Investig. y de Estudios Av. del Inst., Mexico City, Mexico","institution_ids":[]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":[],"corresponding_institution_ids":["https://openalex.org/I68368234"],"apc_list":null,"apc_paid":null,"fwci":0.0,"has_fulltext":false,"cited_by_count":6,"citation_normalized_percentile":{"value":0.15494142,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":{"min":89,"max":96},"biblio":{"volume":null,"issue":null,"first_page":"391","last_page":"394"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T10024","display_name":"TiO2 Photocatalysis and Solar Cells","score":0.9998999834060669,"subfield":{"id":"https://openalex.org/subfields/2105","display_name":"Renewable Energy, Sustainability and the Environment"},"field":{"id":"https://openalex.org/fields/21","display_name":"Energy"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T10024","display_name":"TiO2 Photocatalysis and Solar Cells","score":0.9998999834060669,"subfield":{"id":"https://openalex.org/subfields/2105","display_name":"Renewable Energy, Sustainability and the Environment"},"field":{"id":"https://openalex.org/fields/21","display_name":"Energy"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10078","display_name":"Advanced Photocatalysis Techniques","score":0.9997000098228455,"subfield":{"id":"https://openalex.org/subfields/2105","display_name":"Renewable Energy, Sustainability and the Environment"},"field":{"id":"https://openalex.org/fields/21","display_name":"Energy"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10192","display_name":"Catalytic Processes in Materials Science","score":0.9993000030517578,"subfield":{"id":"https://openalex.org/subfields/2505","display_name":"Materials Chemistry"},"field":{"id":"https://openalex.org/fields/25","display_name":"Materials Science"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/anatase","display_name":"Anatase","score":0.6989470720291138},{"id":"https://openalex.org/keywords/materials-science","display_name":"Materials science","score":0.676365852355957},{"id":"https://openalex.org/keywords/scherrer-equation","display_name":"Scherrer equation","score":0.6694977879524231},{"id":"https://openalex.org/keywords/crystallite","display_name":"Crystallite","score":0.6549270153045654},{"id":"https://openalex.org/keywords/scanning-electron-microscope","display_name":"Scanning electron microscope","score":0.635016679763794},{"id":"https://openalex.org/keywords/analytical-chemistry","display_name":"Analytical Chemistry (journal)","score":0.5907785296440125},{"id":"https://openalex.org/keywords/transmission-electron-microscopy","display_name":"Transmission electron microscopy","score":0.5365005135536194},{"id":"https://openalex.org/keywords/particle-size","display_name":"Particle size","score":0.5143126249313354},{"id":"https://openalex.org/keywords/dissolution","display_name":"Dissolution","score":0.4771965444087982},{"id":"https://openalex.org/keywords/nuclear-chemistry","display_name":"Nuclear chemistry","score":0.4245074987411499},{"id":"https://openalex.org/keywords/precipitation","display_name":"Precipitation","score":0.41588959097862244},{"id":"https://openalex.org/keywords/titanium-dioxide","display_name":"Titanium dioxide","score":0.41493889689445496},{"id":"https://openalex.org/keywords/mineralogy","display_name":"Mineralogy","score":0.35509780049324036},{"id":"https://openalex.org/keywords/chemical-engineering","display_name":"Chemical engineering","score":0.2629730701446533},{"id":"https://openalex.org/keywords/metallurgy","display_name":"Metallurgy","score":0.19666039943695068},{"id":"https://openalex.org/keywords/chromatography","display_name":"Chromatography","score":0.17604407668113708},{"id":"https://openalex.org/keywords/chemistry","display_name":"Chemistry","score":0.16692590713500977},{"id":"https://openalex.org/keywords/composite-material","display_name":"Composite material","score":0.13504058122634888},{"id":"https://openalex.org/keywords/nanotechnology","display_name":"Nanotechnology","score":0.12916934490203857},{"id":"https://openalex.org/keywords/organic-chemistry","display_name":"Organic chemistry","score":0.06515297293663025}],"concepts":[{"id":"https://openalex.org/C2777402863","wikidata":"https://www.wikidata.org/wiki/Q413357","display_name":"Anatase","level":4,"score":0.6989470720291138},{"id":"https://openalex.org/C192562407","wikidata":"https://www.wikidata.org/wiki/Q228736","display_name":"Materials science","level":0,"score":0.676365852355957},{"id":"https://openalex.org/C26940781","wikidata":"https://www.wikidata.org/wiki/Q906979","display_name":"Scherrer equation","level":3,"score":0.6694977879524231},{"id":"https://openalex.org/C137637335","wikidata":"https://www.wikidata.org/wiki/Q899604","display_name":"Crystallite","level":2,"score":0.6549270153045654},{"id":"https://openalex.org/C26771246","wikidata":"https://www.wikidata.org/wiki/Q321095","display_name":"Scanning electron microscope","level":2,"score":0.635016679763794},{"id":"https://openalex.org/C113196181","wikidata":"https://www.wikidata.org/wiki/Q485223","display_name":"Analytical Chemistry (journal)","level":2,"score":0.5907785296440125},{"id":"https://openalex.org/C146088050","wikidata":"https://www.wikidata.org/wiki/Q744818","display_name":"Transmission electron microscopy","level":2,"score":0.5365005135536194},{"id":"https://openalex.org/C187530423","wikidata":"https://www.wikidata.org/wiki/Q7140503","display_name":"Particle size","level":2,"score":0.5143126249313354},{"id":"https://openalex.org/C88380143","wikidata":"https://www.wikidata.org/wiki/Q416674","display_name":"Dissolution","level":2,"score":0.4771965444087982},{"id":"https://openalex.org/C13965031","wikidata":"https://www.wikidata.org/wiki/Q243545","display_name":"Nuclear chemistry","level":1,"score":0.4245074987411499},{"id":"https://openalex.org/C107054158","wikidata":"https://www.wikidata.org/wiki/Q25257","display_name":"Precipitation","level":2,"score":0.41588959097862244},{"id":"https://openalex.org/C2777593239","wikidata":"https://www.wikidata.org/wiki/Q193521","display_name":"Titanium dioxide","level":2,"score":0.41493889689445496},{"id":"https://openalex.org/C199289684","wikidata":"https://www.wikidata.org/wiki/Q83353","display_name":"Mineralogy","level":1,"score":0.35509780049324036},{"id":"https://openalex.org/C42360764","wikidata":"https://www.wikidata.org/wiki/Q83588","display_name":"Chemical engineering","level":1,"score":0.2629730701446533},{"id":"https://openalex.org/C191897082","wikidata":"https://www.wikidata.org/wiki/Q11467","display_name":"Metallurgy","level":1,"score":0.19666039943695068},{"id":"https://openalex.org/C43617362","wikidata":"https://www.wikidata.org/wiki/Q170050","display_name":"Chromatography","level":1,"score":0.17604407668113708},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.16692590713500977},{"id":"https://openalex.org/C159985019","wikidata":"https://www.wikidata.org/wiki/Q181790","display_name":"Composite material","level":1,"score":0.13504058122634888},{"id":"https://openalex.org/C171250308","wikidata":"https://www.wikidata.org/wiki/Q11468","display_name":"Nanotechnology","level":1,"score":0.12916934490203857},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.06515297293663025},{"id":"https://openalex.org/C127413603","wikidata":"https://www.wikidata.org/wiki/Q11023","display_name":"Engineering","level":0,"score":0.0},{"id":"https://openalex.org/C161790260","wikidata":"https://www.wikidata.org/wiki/Q82264","display_name":"Catalysis","level":2,"score":0.0},{"id":"https://openalex.org/C65165184","wikidata":"https://www.wikidata.org/wiki/Q218831","display_name":"Photocatalysis","level":3,"score":0.0},{"id":"https://openalex.org/C121332964","wikidata":"https://www.wikidata.org/wiki/Q413","display_name":"Physics","level":0,"score":0.0},{"id":"https://openalex.org/C153294291","wikidata":"https://www.wikidata.org/wiki/Q25261","display_name":"Meteorology","level":1,"score":0.0}],"mesh":[],"locations_count":1,"locations":[{"id":"doi:10.1109/iceee.2013.6676015","is_oa":false,"landing_page_url":"https://doi.org/10.1109/iceee.2013.6676015","pdf_url":null,"source":null,"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"2013 10th International Conference on Electrical Engineering, Computing Science and Automatic Control (CCE)","raw_type":"proceedings-article"}],"best_oa_location":null,"sustainable_development_goals":[{"score":0.6000000238418579,"display_name":"Clean water and sanitation","id":"https://metadata.un.org/sdg/6"}],"awards":[],"funders":[{"id":"https://openalex.org/F4320321739","display_name":"Consejo Nacional de Ciencia y Tecnolog\u00eda","ror":"https://ror.org/059ex5q34"},{"id":"https://openalex.org/F4320335331","display_name":"Centro de Investigaci\u00f3n y de Estudios Avanzados del Instituto Polit\u00e9cnico Nacional","ror":"https://ror.org/059sp8j34"}],"has_content":{"grobid_xml":false,"pdf":false},"content_urls":null,"referenced_works_count":27,"referenced_works":["https://openalex.org/W602805189","https://openalex.org/W1828065973","https://openalex.org/W1966622518","https://openalex.org/W1978427947","https://openalex.org/W2004996696","https://openalex.org/W2016099549","https://openalex.org/W2020074118","https://openalex.org/W2028455000","https://openalex.org/W2053958193","https://openalex.org/W2060429741","https://openalex.org/W2077822985","https://openalex.org/W2078119797","https://openalex.org/W2079824146","https://openalex.org/W2089501016","https://openalex.org/W2091633783","https://openalex.org/W2099979782","https://openalex.org/W2119585240","https://openalex.org/W2184987089","https://openalex.org/W2272167319","https://openalex.org/W2390700109","https://openalex.org/W2951896472","https://openalex.org/W3046638110","https://openalex.org/W3049485331","https://openalex.org/W3100495642","https://openalex.org/W4285719527","https://openalex.org/W6675211495","https://openalex.org/W6686762310"],"related_works":["https://openalex.org/W1982228173","https://openalex.org/W2984626062","https://openalex.org/W2736164810","https://openalex.org/W4297022385","https://openalex.org/W1965507487","https://openalex.org/W2503894940","https://openalex.org/W4387735882","https://openalex.org/W2916199555","https://openalex.org/W4389565112","https://openalex.org/W2011230153"],"abstract_inverted_index":{"Titanium":[0],"dioxide":[1],"(TiO":[2],"<sub":[3],"xmlns:mml=\"http://www.w3.org/1998/Math/MathML\"":[4],"xmlns:xlink=\"http://www.w3.org/1999/xlink\">2</sub>":[5],")":[6],"nanoparticles":[7],"were":[8,102,122],"synthesized":[9],"by":[10,26,124,156,188],"the":[11,100,138,142,148,151,158],"homogeneous":[12],"precipitation":[13],"method":[14],"using":[15,157],"titanium":[16,31],"(IV)":[17,32],"butoxide":[18,33],"as":[19],"Ti":[20],"precursor.":[21],"The":[22,74,171,183],"solution":[23],"was":[24,63,77,154,186],"prepared":[25],"dissolving":[27],"26":[28],"ml":[29],"of":[30,37,144,166],"in":[34,107,163],"a":[35,58,108,175,180],"mix":[36],"ethanol,":[38],"glacial":[39],"acetic":[40],"acid,":[41],"and":[42,66,83,89,95,117,132,190],"sulfuric":[43],"acid":[44],"(53:43:4":[45],"ml,":[46],"volume":[47],"proportion),":[48],"under":[49],"constant":[50],"magnetic":[51],"stirring":[52],"at":[53,69,80,104,112],"55":[54],"\u00b0C,":[55],"until":[56],"having":[57],"white":[59],"precipitate.":[60],"This":[61],"precipitate":[62],"centrifuged,":[64],"decanted,":[65],"finally":[67],"dried":[68],"100\u00b0C":[70],"for":[71,92],"two":[72],"hours.":[73],"resultant":[75],"product":[76],"thermally":[78],"annealed":[79],"different":[81,113],"temperatures":[82],"times,":[84,114],"namely,":[85],"450,":[86],"550,":[87],"600,":[88],"650":[90],"\u00b0C":[91],"6,":[93],"12":[94],"24":[96],"h,":[97],"respectively.":[98],"Finally":[99],"powders":[101,121],"milled":[103],"400":[105],"rpm":[106],"planetary":[109],"ball":[110],"milling":[111],"2,":[115],"6":[116],"8":[118],"h.":[119],"All":[120,137],"characterized":[123],"X-ray":[125,139],"diffraction":[126],"(XRD),":[127],"Scanning":[128],"Electron":[129,134],"Microscopy":[130,135],"(SEM)":[131],"Transmission":[133],"(TEM).":[136],"spectra":[140],"confirmed":[141],"existence":[143],"anatase":[145],"phase.":[146],"From":[147],"XRD":[149],"spectra,":[150],"crystallites":[152],"size":[153,185],"estimated":[155],"Scherrer's":[159],"fomula,":[160],"giving":[161],"values":[162],"an":[164],"interval":[165],"18":[167],"to":[168,196],"22":[169],"nm.":[170,198],"SEM":[172],"micrographs":[173],"showed":[174],"uniform":[176],"particle":[177,184],"distribution,":[178],"with":[179],"spherical":[181],"shape.":[182],"measured":[187],"TEM":[189],"SEM,":[191],"which":[192],"oscillated":[193],"from":[194],"20":[195],"35":[197]},"counts_by_year":[{"year":2024,"cited_by_count":1},{"year":2023,"cited_by_count":1},{"year":2021,"cited_by_count":1},{"year":2020,"cited_by_count":2},{"year":2017,"cited_by_count":1}],"updated_date":"2026-06-26T08:34:08.712188","created_date":"2025-10-10T00:00:00"}