{"id":"https://openalex.org/W7225375230","doi":"https://doi.org/10.1021/acs.jchemed.6c01288","title":"An Inquiry-Driven Introductory Experiment for the Advanced Organic Chemistry Laboratory to Refresh Students on Fundamental Laboratory Techniques","display_name":"An Inquiry-Driven Introductory Experiment for the Advanced Organic Chemistry Laboratory to Refresh Students on Fundamental Laboratory Techniques","publication_year":2026,"publication_date":"2026-11-06","ids":{"openalex":"https://openalex.org/W7225375230","doi":"https://doi.org/10.1021/acs.jchemed.6c01288"},"language":"en","primary_location":{"id":"doi:10.1021/acs.jchemed.6c01288","doi":"https://doi.org/10.1021/acs.jchemed.6c01288","is_oa":false,"landing_page_url":"https://doi.org/10.1021/acs.jchemed.6c01288","pdf_url":null,"source":{"id":"https://openalex.org/S105208853","display_name":"Journal of Chemical Education","issn_l":"0021-9584","issn":["0021-9584","1938-1328"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-c","erih-plus","jufo-1","ki-jl-1","norway-1","poland-70","russia-white-list-1"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Chemical Education","raw_type":"journal-article"},"volume":null,"type":"article","is_traditional":true,"indexed_in":["crossref"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5126142107","display_name":"Jackson C. Orr","orcid":"https://orcid.org/0009-0009-9728-6001","observed_orcids":["https://orcid.org/0009-0009-9728-6001"]},"institutions":[{"id":"https://openalex.org/I130238516","display_name":"University of Minnesota","ror":"https://ror.org/017zqws13","country_code":"US","type":"education","lineage":["https://openalex.org/I130238516"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Jackson C. Orr","raw_affiliation_strings":["University of Minnesota , , , ,"],"raw_orcid":"https://orcid.org/0009-0009-9728-6001","affiliations":[{"raw_affiliation_string":"University of Minnesota , , , ,","institution_ids":["https://openalex.org/I130238516"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5063714990","display_name":"William J. Howitz","orcid":"https://orcid.org/0000-0001-6323-7126","observed_orcids":["https://orcid.org/0000-0001-6323-7126"]},"institutions":[{"id":"https://openalex.org/I130238516","display_name":"University of Minnesota","ror":"https://ror.org/017zqws13","country_code":"US","type":"education","lineage":["https://openalex.org/I130238516"]}],"countries":["US"],"is_corresponding":true,"raw_author_name":"William J. Howitz","raw_affiliation_strings":["University of Minnesota , , , ,"],"raw_orcid":"https://orcid.org/0000-0001-6323-7126","affiliations":[{"raw_affiliation_string":"University of Minnesota , , , ,","institution_ids":["https://openalex.org/I130238516"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":["https://openalex.org/A5063714990"],"corresponding_institution_ids":["https://openalex.org/I130238516"],"apc_list":{"value":4500,"currency":"USD","value_usd":4500},"apc_paid":null,"fwci":0.0,"has_fulltext":false,"cited_by_count":0,"citation_normalized_percentile":{"value":0.0,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":null,"biblio":{"volume":null,"issue":null,"first_page":null,"last_page":null},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T12327","display_name":"Various Chemistry Research Topics","score":0.9976000189781189,"subfield":{"id":"https://openalex.org/subfields/3304","display_name":"Education"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},"topics":[{"id":"https://openalex.org/T12327","display_name":"Various Chemistry Research Topics","score":0.9976000189781189,"subfield":{"id":"https://openalex.org/subfields/3304","display_name":"Education"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},{"id":"https://openalex.org/T14097","display_name":"Chemistry Education and Research","score":0.0010999999940395355,"subfield":{"id":"https://openalex.org/subfields/3304","display_name":"Education"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},{"id":"https://openalex.org/T10072","display_name":"Science Education and Pedagogy","score":0.0006000000284984708,"subfield":{"id":"https://openalex.org/subfields/3304","display_name":"Education"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/organic-chemistry-laboratory-techniques","display_name":"organic chemistry laboratory techniques","score":0.8399999737739563},{"id":"https://openalex.org/keywords/structure-elucidation","display_name":"structure elucidation","score":0.6600000262260437},{"id":"https://openalex.org/keywords/acid-base-extraction","display_name":"acid-base extraction","score":0.8859999775886536},{"id":"https://openalex.org/keywords/column-chromatography","display_name":"column chromatography","score":0.9980000257492065},{"id":"https://openalex.org/keywords/p-hydroxybenzoic-acid","display_name":"p-hydroxybenzoic acid","score":0.824999988079071},{"id":"https://openalex.org/keywords/nmr-spectroscopy","display_name":"NMR spectroscopy","score":0.6740000247955322},{"id":"https://openalex.org/keywords/gas-chromatography-mass-spectrometry","display_name":"gas chromatography-mass spectrometry","score":0.9200000166893005},{"id":"https://openalex.org/keywords/infrared-spectroscopy","display_name":"infrared spectroscopy","score":0.828000009059906}],"concepts":[{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.5239999890327454},{"id":"https://openalex.org/C198531522","wikidata":"https://www.wikidata.org/wiki/Q485146","display_name":"Sample (material)","level":2,"score":0.42640000581741333},{"id":"https://openalex.org/C145420912","wikidata":"https://www.wikidata.org/wiki/Q853077","display_name":"Mathematics education","level":1,"score":0.40549999475479126},{"id":"https://openalex.org/C2778576202","wikidata":"https://www.wikidata.org/wiki/Q2540164","display_name":"Sample preparation","level":2,"score":0.38040000200271606},{"id":"https://openalex.org/C41008148","wikidata":"https://www.wikidata.org/wiki/Q21198","display_name":"Computer science","level":0,"score":0.3488999903202057},{"id":"https://openalex.org/C47177190","wikidata":"https://www.wikidata.org/wiki/Q207137","display_name":"Curriculum","level":2,"score":0.3327000141143799},{"id":"https://openalex.org/C113196181","wikidata":"https://www.wikidata.org/wiki/Q485223","display_name":"Analytical Chemistry (journal)","level":2,"score":0.32409998774528503},{"id":"https://openalex.org/C2777552389","wikidata":"https://www.wikidata.org/wiki/Q1962728","display_name":"Course (navigation)","level":2,"score":0.32109999656677246},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.3165000081062317},{"id":"https://openalex.org/C28719098","wikidata":"https://www.wikidata.org/wiki/Q44946","display_name":"Point (geometry)","level":2,"score":0.31450000405311584},{"id":"https://openalex.org/C2985358483","wikidata":"https://www.wikidata.org/wiki/Q174211","display_name":"Organic chemicals","level":2,"score":0.2777999937534332},{"id":"https://openalex.org/C13530604","wikidata":"https://www.wikidata.org/wiki/Q15318","display_name":"Melting point","level":2,"score":0.2757999897003174},{"id":"https://openalex.org/C88610354","wikidata":"https://www.wikidata.org/wiki/Q1813494","display_name":"Teaching method","level":2,"score":0.27489998936653137},{"id":"https://openalex.org/C18762648","wikidata":"https://www.wikidata.org/wiki/Q42213","display_name":"Work (physics)","level":2,"score":0.2590999901294708},{"id":"https://openalex.org/C2780551164","wikidata":"https://www.wikidata.org/wiki/Q2306599","display_name":"Column (typography)","level":3,"score":0.25360000133514404},{"id":"https://openalex.org/C21880701","wikidata":"https://www.wikidata.org/wiki/Q2144042","display_name":"Process engineering","level":1,"score":0.25200000405311584}],"mesh":[],"locations_count":1,"locations":[{"id":"doi:10.1021/acs.jchemed.6c01288","doi":"https://doi.org/10.1021/acs.jchemed.6c01288","is_oa":false,"landing_page_url":"https://doi.org/10.1021/acs.jchemed.6c01288","pdf_url":null,"source":{"id":"https://openalex.org/S105208853","display_name":"Journal of Chemical Education","issn_l":"0021-9584","issn":["0021-9584","1938-1328"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-c","erih-plus","jufo-1","ki-jl-1","norway-1","poland-70","russia-white-list-1"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Chemical Education","raw_type":"journal-article"}],"best_oa_location":null,"sustainable_development_goals":[{"score":0.4156000018119812,"display_name":"Quality education","id":"https://metadata.un.org/sdg/4"}],"study_designs":[],"awards":[],"funders":[],"has_content":{"grobid_xml":false,"pdf":false},"content_urls":null,"referenced_works_count":25,"referenced_works":["https://openalex.org/W1964642525","https://openalex.org/W1996135480","https://openalex.org/W2016774599","https://openalex.org/W2035060180","https://openalex.org/W2045103575","https://openalex.org/W2050724700","https://openalex.org/W2061064010","https://openalex.org/W2076007992","https://openalex.org/W2081706168","https://openalex.org/W2086242020","https://openalex.org/W2088817874","https://openalex.org/W2090059359","https://openalex.org/W2150742483","https://openalex.org/W2301459704","https://openalex.org/W2891569903","https://openalex.org/W2969056635","https://openalex.org/W2999129060","https://openalex.org/W3108800138","https://openalex.org/W3172749283","https://openalex.org/W4285727794","https://openalex.org/W4324130777","https://openalex.org/W4381490193","https://openalex.org/W4386274412","https://openalex.org/W4406375307","https://openalex.org/W7131364243"],"related_works":["https://openalex.org/W2007004281","https://openalex.org/W2062102384","https://openalex.org/W7140546243","https://openalex.org/W3194026794","https://openalex.org/W1978939620","https://openalex.org/W2997731523","https://openalex.org/W4401631022","https://openalex.org/W2320181505","https://openalex.org/W2034385582","https://openalex.org/W2081706168"],"abstract_inverted_index":{"Abstract":[0],"Several":[1],"fundamental":[2,62],"organic":[3,12,42,95],"chemistry":[4,13,43],"laboratory":[5,14,29,44,163],"techniques":[6],"are":[7],"introduced":[8],"in":[9,27,168,201],"the":[10,19,54,61,70,74,109,120,150,158,170,182,192,202],"lower-division":[11,55,193],"courses,":[15],"and":[16,31,97,108,122,132,143,173,195],"they":[17,147],"form":[18],"basis":[20],"for":[21,69,116,197],"synthetic":[22],"work":[23],"students":[24,59,165],"might":[25],"encounter":[26],"future":[28],"courses":[30],"research":[32],"experiences.":[33],"For":[34],"those":[35],"going":[36],"on":[37,60,157],"to":[38,184],"take":[39],"an":[40,66,93],"upper-division":[41,71,203],"course":[45,72,194],"offering,":[46],"several":[47],"semesters":[48],"may":[49],"have":[50],"elapsed":[51],"since":[52],"taking":[53],"equivalent.":[56],"To":[57],"refresh":[58],"techniques,":[63],"we":[64],"designed":[65],"introductory":[67],"experiment":[68,183],"involving":[73],"open-ended":[75],"structure":[76,151],"elucidation":[77],"of":[78,87,92,119,124,152,160,189],"a":[79,88,117,161,186],"trisubstituted":[80],"benzene":[81],"derivative.":[82],"Students":[83,179],"receive":[84],"two":[85],"samples":[86],"1:1":[89],"w/w":[90],"mixture":[91],"unknown":[94,154,171],"compound":[96,172],"4-hydroxybenzoic":[98],"acid.":[99],"They":[100],"must":[101],"purify":[102],"one":[103],"sample":[104,111],"using":[105,112,128],"acid\u2013base":[106],"extraction":[107],"other":[110],"column":[113],"chromatography,":[114],"allowing":[115],"comparison":[118],"efficacy":[121],"efficiency":[123],"each":[125],"technique.":[126],"Finally,":[127],"data":[129],"from":[130,191],"1H":[131],"13C":[133],"nuclear":[134],"magnetic":[135],"resonance":[136],"spectroscopy,":[137,139],"infrared":[138],"gas":[140],"chromatography\u2013mass":[141],"spectrometry,":[142],"melting":[144],"point":[145],"analysis,":[146],"can":[148],"elucidate":[149],"their":[153,175,198],"compound.":[155],"Based":[156],"results":[159],"written":[162],"report,":[164],"demonstrated":[166],"proficiency":[167],"identifying":[169],"articulating":[174],"corresponding":[176],"deductive":[177],"logic.":[178],"also":[180],"found":[181],"be":[185],"helpful":[187],"review":[188],"concepts":[190],"beneficial":[196],"success":[199],"later":[200],"course.":[204]},"counts_by_year":[],"updated_date":"2026-11-08T12:12:28.789561","created_date":"2026-11-07T00:00:00"}