{"id":"https://openalex.org/W7217795239","doi":null,"title":"Synthesis and Characterization of 2-bromo-4,5-dimethoxybenzaldehyde Compound from Veratraldehyde and KBrO3 In Situ","display_name":"Synthesis and Characterization of 2-bromo-4,5-dimethoxybenzaldehyde Compound from Veratraldehyde and KBrO3 In Situ","publication_year":2024,"publication_date":"2024-03-20","ids":{"openalex":"https://openalex.org/W7217795239"},"language":"en","primary_location":{"id":"pmh:oai:ojs2.sunankalijaga.org:article/1097","doi":null,"is_oa":true,"landing_page_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/view/1097","pdf_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/download/1097/1075","source":{"id":"https://openalex.org/S4387281041","display_name":"Proceeding International Conference on Religion Science and Education","issn_l":"2828-8467","issn":["2828-8467","2829-3355"],"is_oa":true,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":null,"host_organization_name":null,"host_organization_lineage":[],"host_organization_lineage_names":[],"type":"journal"},"license":"cc-by","license_id":"https://openalex.org/licenses/cc-by","version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"2829-3355","raw_type":"info:eu-repo/semantics/article"},"volume":null,"type":"article","is_traditional":true,"indexed_in":[],"open_access":{"is_oa":true,"oa_status":"diamond","oa_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/download/1097/1075","any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5092558379","display_name":"Khoirotun Nafillah","orcid":"https://orcid.org/0009-0001-0235-7287","observed_orcids":["https://orcid.org/0009-0001-0235-7287"]},"institutions":[{"id":"https://openalex.org/I4405274780","display_name":"Politeknik Maritim Negeri Indonesia","ror":"https://ror.org/02b6kg957","country_code":"ID","type":"education","lineage":["https://openalex.org/I4405274780"]}],"countries":["ID"],"is_corresponding":true,"raw_author_name":"Nafillah, Khoirotun","raw_affiliation_strings":["Politeknik Maritim Negeri Indonesia"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Politeknik Maritim Negeri Indonesia","institution_ids":["https://openalex.org/I4405274780"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":["https://openalex.org/A5092558379"],"corresponding_institution_ids":["https://openalex.org/I4405274780"],"apc_list":null,"apc_paid":null,"fwci":0.0,"has_fulltext":true,"cited_by_count":0,"citation_normalized_percentile":{"value":0.0,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":null,"biblio":{"volume":null,"issue":null,"first_page":null,"last_page":null},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T11831","display_name":"Chemical Synthesis and Reactions","score":0.7778000235557556,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T11831","display_name":"Chemical Synthesis and Reactions","score":0.7778000235557556,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T11989","display_name":"Oxidative Organic Chemistry Reactions","score":0.08990000188350677,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T11746","display_name":"Inorganic and Organometallic Chemistry","score":0.026000000536441803,"subfield":{"id":"https://openalex.org/subfields/1604","display_name":"Inorganic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/veratraldehyde","display_name":"veratraldehyde","score":0.9829999804496765},{"id":"https://openalex.org/keywords/potassium-bromate","display_name":"potassium bromate","score":0.8460000157356262},{"id":"https://openalex.org/keywords/bromination","display_name":"bromination","score":0.8050000071525574},{"id":"https://openalex.org/keywords/electrophilic-aromatic-substitution","display_name":"electrophilic aromatic substitution","score":0.984000027179718},{"id":"https://openalex.org/keywords/scale-up","display_name":"scale-up","score":0.5019999742507935},{"id":"https://openalex.org/keywords/substituted-benzaldehydes","display_name":"benzaldehyde derivatives","score":0.7279999852180481}],"concepts":[{"id":"https://openalex.org/C65973085","wikidata":"https://www.wikidata.org/wiki/Q888529","display_name":"Halogenation","level":2,"score":0.8722000122070312},{"id":"https://openalex.org/C77176794","wikidata":"https://www.wikidata.org/wiki/Q187689","display_name":"Oxidizing agent","level":2,"score":0.7235999703407288},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.7067999839782715},{"id":"https://openalex.org/C2776254738","wikidata":"https://www.wikidata.org/wiki/Q81406","display_name":"Alkene","level":3,"score":0.6809999942779541},{"id":"https://openalex.org/C517835270","wikidata":"https://www.wikidata.org/wiki/Q879","display_name":"Bromine","level":2,"score":0.6467000246047974},{"id":"https://openalex.org/C2779692420","wikidata":"https://www.wikidata.org/wiki/Q372524","display_name":"Benzaldehyde","level":3,"score":0.45660001039505005},{"id":"https://openalex.org/C50027330","wikidata":"https://www.wikidata.org/wiki/Q908086","display_name":"Electrophile","level":3,"score":0.44859999418258667},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.4449000060558319},{"id":"https://openalex.org/C505241676","wikidata":"https://www.wikidata.org/wiki/Q688","display_name":"Chlorine","level":2,"score":0.4056999981403351},{"id":"https://openalex.org/C2780407432","wikidata":"https://www.wikidata.org/wiki/Q103230","display_name":"Ether","level":2,"score":0.3871999979019165},{"id":"https://openalex.org/C2777899863","wikidata":"https://www.wikidata.org/wiki/Q4428995","display_name":"Sorbent","level":3,"score":0.38190001249313354},{"id":"https://openalex.org/C160892712","wikidata":"https://www.wikidata.org/wiki/Q901559","display_name":"Fourier transform infrared spectroscopy","level":2,"score":0.38119998574256897},{"id":"https://openalex.org/C2780841128","wikidata":"https://www.wikidata.org/wiki/Q5073781","display_name":"Characterization (materials science)","level":2,"score":0.3772999942302704},{"id":"https://openalex.org/C21951064","wikidata":"https://www.wikidata.org/wiki/Q899212","display_name":"Combinatorial chemistry","level":1,"score":0.3734000027179718},{"id":"https://openalex.org/C32909587","wikidata":"https://www.wikidata.org/wiki/Q11369","display_name":"Molecule","level":2,"score":0.366100013256073},{"id":"https://openalex.org/C2777965246","wikidata":"https://www.wikidata.org/wiki/Q899587","display_name":"Electrophilic substitution","level":2,"score":0.366100013256073},{"id":"https://openalex.org/C13530604","wikidata":"https://www.wikidata.org/wiki/Q15318","display_name":"Melting point","level":2,"score":0.35120001435279846},{"id":"https://openalex.org/C153642686","wikidata":"https://www.wikidata.org/wiki/Q70906","display_name":"Infrared spectroscopy","level":2,"score":0.336899995803833},{"id":"https://openalex.org/C125287762","wikidata":"https://www.wikidata.org/wiki/Q1758948","display_name":"Absorption (acoustics)","level":2,"score":0.32589998841285706},{"id":"https://openalex.org/C158355884","wikidata":"https://www.wikidata.org/wiki/Q11388","display_name":"Infrared","level":2,"score":0.3165000081062317},{"id":"https://openalex.org/C114373084","wikidata":"https://www.wikidata.org/wiki/Q273499","display_name":"Chemical synthesis","level":3,"score":0.3068999946117401},{"id":"https://openalex.org/C2777332933","wikidata":"https://www.wikidata.org/wiki/Q170409","display_name":"Functional group","level":3,"score":0.3000999987125397},{"id":"https://openalex.org/C162356407","wikidata":"https://www.wikidata.org/wiki/Q180809","display_name":"Mass spectrometry","level":2,"score":0.29820001125335693},{"id":"https://openalex.org/C198440531","wikidata":"https://www.wikidata.org/wiki/Q899027","display_name":"Electrophilic addition","level":4,"score":0.29109999537467957},{"id":"https://openalex.org/C119824511","wikidata":"https://www.wikidata.org/wiki/Q13553575","display_name":"Absorption spectroscopy","level":2,"score":0.27250000834465027},{"id":"https://openalex.org/C535685238","wikidata":"https://www.wikidata.org/wiki/Q1153832","display_name":"Organic synthesis","level":3,"score":0.2712000012397766},{"id":"https://openalex.org/C122085161","wikidata":"https://www.wikidata.org/wiki/Q597833","display_name":"Electrophilic aromatic substitution","level":2,"score":0.27000001072883606},{"id":"https://openalex.org/C188027245","wikidata":"https://www.wikidata.org/wiki/Q750446","display_name":"Polymer chemistry","level":1,"score":0.2678000032901764},{"id":"https://openalex.org/C2779825165","wikidata":"https://www.wikidata.org/wiki/Q101497","display_name":"Aldehyde","level":3,"score":0.25270000100135803},{"id":"https://openalex.org/C2991944050","wikidata":"https://www.wikidata.org/wiki/Q36534","display_name":"Reaction conditions","level":3,"score":0.25040000677108765}],"mesh":[],"locations_count":1,"locations":[{"id":"pmh:oai:ojs2.sunankalijaga.org:article/1097","doi":null,"is_oa":true,"landing_page_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/view/1097","pdf_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/download/1097/1075","source":{"id":"https://openalex.org/S4387281041","display_name":"Proceeding International Conference on Religion Science and Education","issn_l":"2828-8467","issn":["2828-8467","2829-3355"],"is_oa":true,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":null,"host_organization_name":null,"host_organization_lineage":[],"host_organization_lineage_names":[],"type":"journal"},"license":"cc-by","license_id":"https://openalex.org/licenses/cc-by","version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"2829-3355","raw_type":"info:eu-repo/semantics/article"}],"best_oa_location":{"id":"pmh:oai:ojs2.sunankalijaga.org:article/1097","doi":null,"is_oa":true,"landing_page_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/view/1097","pdf_url":"https://sunankalijaga.org/prosiding/index.php/icrse/article/download/1097/1075","source":{"id":"https://openalex.org/S4387281041","display_name":"Proceeding International Conference on Religion Science and Education","issn_l":"2828-8467","issn":["2828-8467","2829-3355"],"is_oa":true,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":null,"host_organization_name":null,"host_organization_lineage":[],"host_organization_lineage_names":[],"type":"journal"},"license":"cc-by","license_id":"https://openalex.org/licenses/cc-by","version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"2829-3355","raw_type":"info:eu-repo/semantics/article"},"sustainable_development_goals":[],"study_designs":[],"awards":[],"funders":[{"id":"https://openalex.org/F4320328515","display_name":"Lembaga Pengelola Dana Pendidikan","ror":"https://ror.org/05p2xef58"}],"has_content":{"pdf":true,"grobid_xml":true},"content_urls":{"pdf":"https://content.openalex.org/works/W7217795239.pdf","grobid_xml":"https://content.openalex.org/works/W7217795239.grobid-xml"},"referenced_works_count":17,"referenced_works":["https://openalex.org/W580825176","https://openalex.org/W1251300728","https://openalex.org/W1968816806","https://openalex.org/W2043797909","https://openalex.org/W2055231536","https://openalex.org/W2058957010","https://openalex.org/W2118845091","https://openalex.org/W2332963840","https://openalex.org/W2401448071","https://openalex.org/W2759092278","https://openalex.org/W2793143301","https://openalex.org/W2951376086","https://openalex.org/W3038029158","https://openalex.org/W4366608227","https://openalex.org/W4367042821","https://openalex.org/W4381050716","https://openalex.org/W4386002461"],"related_works":["https://openalex.org/W2360392496","https://openalex.org/W1965058352","https://openalex.org/W2349636406","https://openalex.org/W1432363413","https://openalex.org/W1991679947","https://openalex.org/W2391465769","https://openalex.org/W2374493152","https://openalex.org/W2348274883","https://openalex.org/W2376499819","https://openalex.org/W95605906"],"abstract_inverted_index":{"Bromination":[0,15],"is":[1,50],"an":[2,18,57],"addition":[3],"reaction":[4,16],"of":[5,26,29,38,75,88,115,143,165,179,187],"bromo":[6],"groups":[7],"in":[8,21,32,89,95,102],"alkene":[9],"double":[10],"bounds":[11],"like":[12],"benzaldehyde":[13],"derivatives.":[14],"has":[17],"important":[19],"role":[20],"the":[22,27,36,76,107,122,130,163,166,204],"industrial":[23],"chemistry":[24],"because":[25],"multifunctionality":[28],"organobromide":[30],"products":[31],"various":[33],"syntheses.":[34],"However,":[35],"use":[37,83],"bromine":[39,55],"molecules":[40],"can":[41],"be":[42],"toxic":[43],"and":[44,71,137,147,157,171],"reactive.":[45],"An":[46],"alternative":[47],"bromination":[48,93],"procedure":[49],"needed":[51],"by":[52],"avoiding":[53],"directly":[54],"through":[56],"oxidizing":[58],"agents":[59],"such":[60],"as":[61,85],"KBrO3.":[62],"This":[63],"research":[64],"aims":[65],"to":[66,105,203],"carry":[67],"out":[68],"synthesis,":[69],"characterization":[70],"scale":[72],"up":[73,119],"study":[74,97,120],"compound":[77,110,123,131],"2-bromo-4,5-dimethoxybenzaldehyde":[78,109,124],"from":[79],"veratraldehyde":[80],"basic":[81],"material":[82],"KBrO3":[84],"a":[86,112,184,194],"source":[87],"situ":[90],"bromine.":[91],"The":[92,149,159,176,190],"mechanism":[94],"this":[96],"used":[98],"electrophilic":[99],"aromatic":[100,170],"substitution":[101],"acidic":[103],"conditions":[104],"produce":[106],"gray-white":[108],"with":[111,140,198],"melting":[113],"point":[114],"142-144":[116],"\u00b0C.":[117],"Scale":[118],"on":[121,129],"showed":[125,162,193],"that":[126],"mass":[127,191],"variations":[128],"veratraldehyde,":[132],"namely":[133],"0.5;":[134],"1.0;":[135],"2.0;":[136],"3.0":[138],"grams":[139],"successive":[141],"yields":[142],"21.63;":[144],"82.03;":[145],"69.38;":[146],"69.84%.":[148],"synthesis":[150],"results":[151],"were":[152],"characterized":[153],"using":[154],"TLC,":[155],"FTIR,":[156],"GC-MS.":[158],"FTIR":[160],"spectrum":[161,192],"vibration":[164],"C-Br,":[167],"C=O,":[168],"C=C":[169],"C-O":[172],"ether":[173],"functional":[174],"groups.":[175],"typical":[177],"absorption":[178,182],"C-Br":[180],"shows":[181],"at":[183],"wave":[185],"number":[186],"1018":[188],"cm-1.":[189],"molecular":[195],"ion":[196],"(M+)":[197],"m/z":[199],"244":[200],"which":[201],"corresponds":[202],"target":[205],"molecule.":[206]},"counts_by_year":[],"updated_date":"2026-11-07T11:25:07.637180","created_date":"2026-10-03T00:00:00"}