{"id":"https://openalex.org/W4386983995","doi":"https://doi.org/10.1093/jaoacint/qsad111","title":"Optimization of a Solid-Phase Extraction Coupled with a High-Performance Liquid Chromatography and Diode Array Ultraviolet Detection Method for Monitoring of Different Antibiotic Class Residues in Water Samples","display_name":"Optimization of a Solid-Phase Extraction Coupled with a High-Performance Liquid Chromatography and Diode Array Ultraviolet Detection Method for Monitoring of Different Antibiotic Class Residues in Water Samples","publication_year":2023,"publication_date":"2023-09-22","ids":{"openalex":"https://openalex.org/W4386983995","doi":"https://doi.org/10.1093/jaoacint/qsad111","pmid":"https://pubmed.ncbi.nlm.nih.gov/37740954"},"language":"en","primary_location":{"id":"doi:10.1093/jaoacint/qsad111","doi":"https://doi.org/10.1093/jaoacint/qsad111","is_oa":true,"landing_page_url":"https://doi.org/10.1093/jaoacint/qsad111","pdf_url":"https://academic.oup.com/jaoac/advance-article-pdf/doi/10.1093/jaoacint/qsad111/52431819/qsad111.pdf","source":{"id":"https://openalex.org/S103486911","display_name":"Journal of AOAC International","issn_l":"1060-3271","issn":["1060-3271","1944-7922"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-b","jufo-1","medline","norway-1","poland-40","russia-white-list-2","vabb-shw"],"host_organization":"https://openalex.org/P4310311648","host_organization_name":"Oxford University Press","host_organization_lineage":["https://openalex.org/P4310311648","https://openalex.org/P4310311647"],"host_organization_lineage_names":["Oxford University Press","University of Oxford"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC International","raw_type":"journal-article"},"volume":null,"type":"article","is_traditional":true,"indexed_in":["crossref","pubmed"],"open_access":{"is_oa":true,"oa_status":"bronze","oa_url":"https://academic.oup.com/jaoac/advance-article-pdf/doi/10.1093/jaoacint/qsad111/52431819/qsad111.pdf","any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5108390882","display_name":"Rania A Mahmoud","orcid":"https://orcid.org/0009-0006-0063-2819","observed_orcids":["https://orcid.org/0009-0006-0063-2819"]},"institutions":[],"countries":[],"is_corresponding":false,"raw_author_name":"Rania A Mahmoud","raw_affiliation_strings":["Medical Union Pharmaceuticals Co., R&D-Methodology and Stability Department , Abu Sultan, Ismailia, 41617, Egypt"],"raw_orcid":"https://orcid.org/0009-0006-0063-2819","affiliations":[{"raw_affiliation_string":"Medical Union Pharmaceuticals Co., R&D-Methodology and Stability Department , Abu Sultan, Ismailia, 41617, Egypt","institution_ids":[]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5041119221","display_name":"Ghada M. Hadad","orcid":"https://orcid.org/0000-0003-1386-5401","observed_orcids":["https://orcid.org/0000-0003-1386-5401"]},"institutions":[{"id":"https://openalex.org/I114794399","display_name":"Suez Canal University","ror":"https://ror.org/02m82p074","country_code":"EG","type":"education","lineage":["https://openalex.org/I114794399"]}],"countries":["EG"],"is_corresponding":false,"raw_author_name":"Ghada M Hadad","raw_affiliation_strings":["Suez Canal University, Faculty of Pharmacy, Pharmaceutical Analytical Chemistry Department, Ismailia, 41522, Egypt"],"raw_orcid":"https://orcid.org/0000-0003-1386-5401","affiliations":[{"raw_affiliation_string":"Suez Canal University, Faculty of Pharmacy, Pharmaceutical Analytical Chemistry Department, Ismailia, 41522, Egypt","institution_ids":["https://openalex.org/I114794399"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5018586571","display_name":"Randa A. Abdel Salam","orcid":"https://orcid.org/0000-0001-7554-3577","observed_orcids":["https://orcid.org/0000-0001-7554-3577"]},"institutions":[{"id":"https://openalex.org/I114794399","display_name":"Suez Canal University","ror":"https://ror.org/02m82p074","country_code":"EG","type":"education","lineage":["https://openalex.org/I114794399"]}],"countries":["EG"],"is_corresponding":false,"raw_author_name":"Randa A Abdel Salam","raw_affiliation_strings":["Suez Canal University, Faculty of Pharmacy, Pharmaceutical Analytical Chemistry Department, Ismailia, 41522, Egypt"],"raw_orcid":"https://orcid.org/0000-0001-7554-3577","affiliations":[{"raw_affiliation_string":"Suez Canal University, Faculty of Pharmacy, Pharmaceutical Analytical Chemistry Department, Ismailia, 41522, Egypt","institution_ids":["https://openalex.org/I114794399"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5066606731","display_name":"Hatem I. Mokhtar","orcid":"https://orcid.org/0000-0002-9337-1809","observed_orcids":["https://orcid.org/0000-0002-9337-1809"]},"institutions":[{"id":"https://openalex.org/I1355163","display_name":"Sinai University","ror":"https://ror.org/01dd13a92","country_code":"EG","type":"education","lineage":["https://openalex.org/I1355163"]}],"countries":["EG"],"is_corresponding":true,"raw_author_name":"Hatem I Mokhtar","raw_affiliation_strings":["Sinai University-Kantara Branch, Faculty of Pharmacy, Pharmaceutical Chemistry Department, 41636, Egypt"],"raw_orcid":"https://orcid.org/0000-0002-9337-1809","affiliations":[{"raw_affiliation_string":"Sinai University-Kantara Branch, Faculty of Pharmacy, Pharmaceutical Chemistry Department, 41636, Egypt","institution_ids":["https://openalex.org/I1355163"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":2,"corresponding_author_ids":["https://openalex.org/A5066606731"],"corresponding_institution_ids":["https://openalex.org/I1355163"],"apc_list":{"value":1711,"currency":"USD","value_usd":1711},"apc_paid":null,"fwci":1.0167,"has_fulltext":true,"cited_by_count":16,"citation_normalized_percentile":{"value":0.67987143,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":{"min":95,"max":99},"biblio":{"volume":"107","issue":"1","first_page":"52","last_page":"60"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T10419","display_name":"Pharmaceutical and Antibiotic Environmental Impacts","score":0.614300012588501,"subfield":{"id":"https://openalex.org/subfields/2310","display_name":"Pollution"},"field":{"id":"https://openalex.org/fields/23","display_name":"Environmental Science"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T10419","display_name":"Pharmaceutical and Antibiotic Environmental Impacts","score":0.614300012588501,"subfield":{"id":"https://openalex.org/subfields/2310","display_name":"Pollution"},"field":{"id":"https://openalex.org/fields/23","display_name":"Environmental Science"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T11423","display_name":"Pesticide Residue Analysis and Safety","score":0.1298999935388565,"subfield":{"id":"https://openalex.org/subfields/1106","display_name":"Food Science"},"field":{"id":"https://openalex.org/fields/11","display_name":"Agricultural and Biological Sciences"},"domain":{"id":"https://openalex.org/domains/1","display_name":"Life Sciences"}},{"id":"https://openalex.org/T10180","display_name":"Analytical chemistry methods development","score":0.11829999834299088,"subfield":{"id":"https://openalex.org/subfields/1602","display_name":"Analytical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/antibiotic-residues","display_name":"antibiotic residues","score":0.9509999752044678},{"id":"https://openalex.org/keywords/cephalosporins","display_name":"cephalosporins","score":0.9010000228881836},{"id":"https://openalex.org/keywords/cefotaxime","display_name":"cefotaxime","score":0.8700000047683716},{"id":"https://openalex.org/keywords/ceftriaxone","display_name":"ceftriaxone","score":0.8809999823570251},{"id":"https://openalex.org/keywords/cefoperazone","display_name":"cefoperazone","score":0.878000020980835},{"id":"https://openalex.org/keywords/cefdinir","display_name":"cefdinir","score":0.734000027179718},{"id":"https://openalex.org/keywords/amoxicillin","display_name":"amoxicillin","score":0.9049999713897705},{"id":"https://openalex.org/keywords/levofloxacin","display_name":"levofloxacin","score":0.9919999837875366},{"id":"https://openalex.org/keywords/ciprofloxacin","display_name":"ciprofloxacin","score":0.9990000128746033},{"id":"https://openalex.org/keywords/solid-phase-extraction","display_name":"solid-phase extraction","score":0.9340000152587891},{"id":"https://openalex.org/keywords/hplc-dad","display_name":"HPLC-DAD","score":0.8240000009536743},{"id":"https://openalex.org/keywords/water-pollution","display_name":"water pollution","score":0.5950000286102295},{"id":"https://openalex.org/keywords/hospital-wastewater","display_name":"hospital wastewater","score":0.6980000138282776},{"id":"https://openalex.org/keywords/cleaning-validation","display_name":"cleaning validation","score":0.9129999876022339},{"id":"https://openalex.org/keywords/stainless-steel-surfaces","display_name":"stainless steel surfaces","score":0.6819999814033508},{"id":"https://openalex.org/keywords/environmental-water-monitoring","display_name":"environmental water monitoring","score":0.652999997138977}],"concepts":[{"id":"https://openalex.org/C43617362","wikidata":"https://www.wikidata.org/wiki/Q170050","display_name":"Chromatography","level":1,"score":0.8255626559257507},{"id":"https://openalex.org/C179998833","wikidata":"https://www.wikidata.org/wiki/Q381233","display_name":"High-performance liquid chromatography","level":2,"score":0.7842207551002502},{"id":"https://openalex.org/C81426234","wikidata":"https://www.wikidata.org/wiki/Q1408763","display_name":"Solid phase extraction","level":3,"score":0.6408160924911499},{"id":"https://openalex.org/C119128265","wikidata":"https://www.wikidata.org/wiki/Q900165","display_name":"Detection limit","level":2,"score":0.5117976069450378},{"id":"https://openalex.org/C110084920","wikidata":"https://www.wikidata.org/wiki/Q381624","display_name":"Chromatography detector","level":3,"score":0.47030776739120483},{"id":"https://openalex.org/C2779314605","wikidata":"https://www.wikidata.org/wiki/Q5220980","display_name":"Danofloxacin","level":5,"score":0.4201773703098297},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.4055843949317932},{"id":"https://openalex.org/C192562407","wikidata":"https://www.wikidata.org/wiki/Q228736","display_name":"Materials science","level":0,"score":0.35549649596214294},{"id":"https://openalex.org/C2778512257","wikidata":"https://www.wikidata.org/wiki/Q256602","display_name":"Ciprofloxacin","level":3,"score":0.35270392894744873},{"id":"https://openalex.org/C501593827","wikidata":"https://www.wikidata.org/wiki/Q12187","display_name":"Antibiotics","level":2,"score":0.1714312732219696},{"id":"https://openalex.org/C2779906673","wikidata":"https://www.wikidata.org/wiki/Q414413","display_name":"Enrofloxacin","level":4,"score":0.1246216893196106},{"id":"https://openalex.org/C55493867","wikidata":"https://www.wikidata.org/wiki/Q7094","display_name":"Biochemistry","level":1,"score":0.0}],"mesh":[{"descriptor_ui":"D000900","descriptor_name":"Anti-Bacterial Agents","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":true},{"descriptor_ui":"D002439","descriptor_name":"Cefotaxime","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":false},{"descriptor_ui":"D002511","descriptor_name":"Cephalosporins","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":false},{"descriptor_ui":"D002851","descriptor_name":"Chromatography, High Pressure Liquid","qualifier_ui":"Q000379","qualifier_name":"methods","is_major_topic":false},{"descriptor_ui":"D002853","descriptor_name":"Chromatography, Liquid","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D014867","descriptor_name":"Water","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D052616","descriptor_name":"Solid Phase Extraction","qualifier_ui":"Q000379","qualifier_name":"methods","is_major_topic":false},{"descriptor_ui":"D053719","descriptor_name":"Tandem Mass Spectrometry","qualifier_ui":null,"qualifier_name":null,"is_major_topic":true}],"locations_count":2,"locations":[{"id":"doi:10.1093/jaoacint/qsad111","doi":"https://doi.org/10.1093/jaoacint/qsad111","is_oa":true,"landing_page_url":"https://doi.org/10.1093/jaoacint/qsad111","pdf_url":"https://academic.oup.com/jaoac/advance-article-pdf/doi/10.1093/jaoacint/qsad111/52431819/qsad111.pdf","source":{"id":"https://openalex.org/S103486911","display_name":"Journal of AOAC International","issn_l":"1060-3271","issn":["1060-3271","1944-7922"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-b","jufo-1","medline","norway-1","poland-40","russia-white-list-2","vabb-shw"],"host_organization":"https://openalex.org/P4310311648","host_organization_name":"Oxford University Press","host_organization_lineage":["https://openalex.org/P4310311648","https://openalex.org/P4310311647"],"host_organization_lineage_names":["Oxford University Press","University of Oxford"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC International","raw_type":"journal-article"},{"id":"pmid:37740954","doi":null,"is_oa":false,"landing_page_url":"https://pubmed.ncbi.nlm.nih.gov/37740954","pdf_url":null,"source":{"id":"https://openalex.org/S4306525036","display_name":"PubMed","issn_l":null,"issn":null,"is_oa":false,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":"https://openalex.org/I1299303238","host_organization_name":"National Institutes of Health","host_organization_lineage":["https://openalex.org/I1299303238"],"host_organization_lineage_names":[],"type":"repository"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC International","raw_type":"Journal Article"}],"best_oa_location":{"id":"doi:10.1093/jaoacint/qsad111","doi":"https://doi.org/10.1093/jaoacint/qsad111","is_oa":true,"landing_page_url":"https://doi.org/10.1093/jaoacint/qsad111","pdf_url":"https://academic.oup.com/jaoac/advance-article-pdf/doi/10.1093/jaoacint/qsad111/52431819/qsad111.pdf","source":{"id":"https://openalex.org/S103486911","display_name":"Journal of AOAC International","issn_l":"1060-3271","issn":["1060-3271","1944-7922"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-b","jufo-1","medline","norway-1","poland-40","russia-white-list-2","vabb-shw"],"host_organization":"https://openalex.org/P4310311648","host_organization_name":"Oxford University Press","host_organization_lineage":["https://openalex.org/P4310311648","https://openalex.org/P4310311647"],"host_organization_lineage_names":["Oxford University Press","University of Oxford"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC International","raw_type":"journal-article"},"sustainable_development_goals":[{"display_name":"Clean water and sanitation","score":0.965499997138977,"id":"https://metadata.un.org/sdg/6"},{"display_name":"Good health and well-being","score":0.5683000087738037,"id":"https://metadata.un.org/sdg/3"}],"study_designs":[],"awards":[],"funders":[],"has_content":{"grobid_xml":true,"pdf":true},"content_urls":{"pdf":"https://content.openalex.org/works/W4386983995.pdf","grobid_xml":"https://content.openalex.org/works/W4386983995.grobid-xml"},"referenced_works_count":25,"referenced_works":["https://openalex.org/W1968539350","https://openalex.org/W2030259310","https://openalex.org/W2030512175","https://openalex.org/W2047397655","https://openalex.org/W2047817888","https://openalex.org/W2058634855","https://openalex.org/W2064568876","https://openalex.org/W2077998394","https://openalex.org/W2098955155","https://openalex.org/W2156550863","https://openalex.org/W2442749541","https://openalex.org/W2488942425","https://openalex.org/W2765388348","https://openalex.org/W2768276846","https://openalex.org/W2769682494","https://openalex.org/W2791122350","https://openalex.org/W2902493574","https://openalex.org/W2903002447","https://openalex.org/W2935801545","https://openalex.org/W2944498967","https://openalex.org/W2976711054","https://openalex.org/W3166407278","https://openalex.org/W3171105738","https://openalex.org/W4285087676","https://openalex.org/W4307959123"],"related_works":["https://openalex.org/W2064568876","https://openalex.org/W3141093782","https://openalex.org/W2282412058","https://openalex.org/W2089989085","https://openalex.org/W3206713207","https://openalex.org/W4401665687","https://openalex.org/W2499066190","https://openalex.org/W2765388348","https://openalex.org/W2371300065","https://openalex.org/W2088248453"],"abstract_inverted_index":{"BACKGROUND:":[0],"The":[1,143,174,193,223,267],"increased":[2],"use":[3],"of":[4,17,32,69,114,129,136,140,151,184,188,200,213,216,234,240,263],"cephalosporin":[5,72],"antibiotics":[6],"in":[7,20,87,232,237],"the":[8,15,67,111,115,120,127,130,137,149,198,270],"last":[9],"few":[10],"years":[11],"as":[12,14,244],"well":[13],"detection":[16,60,275],"their":[18,33],"residues":[19,34,68,236],"wastewater":[21,26],"treatment":[22],"plants":[23],"and":[24,43,63,79,85,97,155,167,186,226,247,255,284],"hospital":[25],"poses":[27],"a":[28,98,104,205],"risk":[29],"for":[30,110,182,261,282,290],"infiltration":[31],"into":[35],"environmental":[36,245],"water":[37,88,201,241],"samples.":[38,89],"OBJECTIVE:":[39],"A":[40],"simplified,":[41],"sensitive,":[42],"convenient":[44],"solid-phase":[45],"extraction":[46,128],"(SPE)":[47],"procedure":[48,272],"coupled":[49],"with":[50,57,82,133,153,269],"either":[51],"HPLC":[52,55,100,157,257],"or":[53],"fast":[54,99,112,156,256],"methods":[56,176,258],"diode":[58],"array":[59,93],"was":[61,123,146,195,220],"developed":[62,109,175,260],"validated":[64],"to":[65,125,158,164,170,197,279,287],"screen":[66],"six":[70],"different":[71,238,265],"antibiotics:":[73],"cefoperazone,":[74],"cefipime,":[75],"ceftazedime,":[76],"ceftriaxone,":[77],"cefdinir,":[78],"cefotaxime,":[80],"along":[81],"amoxicillin,":[83],"levofloxacin,":[84],"ciprofloxacin":[86],"METHODS:":[90],"An":[91],"HPLC-diode":[92],"detector":[94],"(HPLC-DAD)":[95],"method":[96,144,194],"method,":[101],"based":[102],"on":[103],"core-shell":[105],"stationary":[106],"phase,":[107],"were":[108,177,259],"screening":[113],"antibiotic":[116,235],"compounds.":[117],"In":[118,208],"addition,":[119],"SPE":[121,152,271],"step":[122],"optimized":[124],"enable":[126],"studied":[131],"drugs":[132],"high":[134,227],"accuracy":[135],"recovered":[138],"amounts":[139],"residues.":[141],"RESULTS:":[142],"sensitivity":[145,228],"enhanced":[147],"by":[148,179],"coupling":[150],"HPLC-DAD":[154,254],"achieve":[159],"low":[160,274],"LODs;":[161],"from":[162,168,204,249,277,285],"0.2":[163,278],"3.8":[165,280],"ng/mL":[166,281,289],"0.65":[169,286],"12.2":[171,288],"ng/mL,":[172],"respectively.":[173],"augmented":[178],"LC-MS/MS":[180],"determination":[181],"confirmation":[183],"identity":[185],"quantity":[187],"any":[189],"positively":[190],"identified":[191],"sample.":[192],"applied":[196],"analysis":[199],"samples":[202,242,246,248],"collected":[203],"rural":[206],"site.":[207],"Addition,":[209],"an":[210],"example":[211],"application":[212,231],"cleaning":[214,250],"validation":[215,251],"cefotaxime-contaminated":[217],"stainless-steel":[218],"surfaces":[219],"provided.":[221],"CONCLUSION:":[222],"method's":[224],"simplicity":[225],"encourage":[229],"its":[230],"monitoring":[233],"types":[239],"such":[243],"activities.":[252],"HIGHLIGHTS:":[253],"separation":[262],"nine":[264],"antibiotics.":[266],"combination":[268],"achieved":[273],"limits;":[276],"SPE-HPLC-DAD":[283],"SPE-fast":[291],"HPLC.":[292]},"counts_by_year":[{"year":2026,"cited_by_count":5},{"year":2025,"cited_by_count":8},{"year":2024,"cited_by_count":3}],"updated_date":"2026-11-04T10:54:05.112534","created_date":"2023-09-24T00:00:00"}
