{"id":"https://openalex.org/W4386700550","doi":"https://doi.org/10.1134/s1061934823090162","title":"Optimization of an Acid-Catalyzed Direct Extraction-Methylation Method of Lipid Residues in Archaeological Vessels by Experimental Design and Response Surface Methodology","display_name":"Optimization of an Acid-Catalyzed Direct Extraction-Methylation Method of Lipid Residues in Archaeological Vessels by Experimental Design and Response Surface Methodology","publication_year":2023,"publication_date":"2023-09-01","ids":{"openalex":"https://openalex.org/W4386700550","doi":"https://doi.org/10.1134/s1061934823090162"},"language":"en","primary_location":{"id":"doi:10.1134/s1061934823090162","doi":"https://doi.org/10.1134/s1061934823090162","is_oa":false,"landing_page_url":"https://doi.org/10.1134/s1061934823090162","pdf_url":null,"source":{"id":"https://openalex.org/S3394804","display_name":"Journal of Analytical Chemistry","issn_l":"0021-8766","issn":["0021-8766","0044-4502","1061-9348","1608-3199","3034-512X"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-d","norway-1","poland-40","russia-white-list-1","russia-white-list-3","vabb-shw"],"host_organization":"https://openalex.org/P4310320267","host_organization_name":"Pleiades Publishing","host_organization_lineage":["https://openalex.org/P4310320267","https://openalex.org/P4310319965"],"host_organization_lineage_names":["Pleiades Publishing","Springer Nature"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Analytical Chemistry","raw_type":"journal-article"},"volume":null,"type":"article","is_traditional":true,"indexed_in":["crossref"],"open_access":{"is_oa":true,"oa_status":"green","oa_url":"https://acikkaynak.bilecik.edu.tr/bitstreams/d03e41c8-6e8d-402c-9ff0-89096d24aa59/download","any_repository_has_fulltext":true},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5005689493","display_name":"\u0130smail Tarhan","orcid":"https://orcid.org/0000-0003-3353-8635","observed_orcids":["https://orcid.org/0000-0003-3353-8635"]},"institutions":[{"id":"https://openalex.org/I137996928","display_name":"Sel\u00e7uk University","ror":"https://ror.org/045hgzm75","country_code":"TR","type":"education","lineage":["https://openalex.org/I137996928"]}],"countries":["TR"],"is_corresponding":true,"raw_author_name":"\u0130smail Tarhan","raw_affiliation_strings":["Sel\u00e7uk University, Faculty of Science, Department of Biochemistry, Konya, Turkey"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Sel\u00e7uk University, Faculty of Science, Department of Biochemistry, Konya, Turkey","institution_ids":["https://openalex.org/I137996928"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5050745380","display_name":"\u015eek\u00fcre \u00c7elikten","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I137996928","display_name":"Sel\u00e7uk University","ror":"https://ror.org/045hgzm75","country_code":"TR","type":"education","lineage":["https://openalex.org/I137996928"]}],"countries":["TR"],"is_corresponding":false,"raw_author_name":"\u015eek\u00fcre \u00c7elikten","raw_affiliation_strings":["Sel\u00e7uk University, Faculty of Science, Department of Biochemistry, Konya, Turkey"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Sel\u00e7uk University, Faculty of Science, Department of Biochemistry, Konya, Turkey","institution_ids":["https://openalex.org/I137996928"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5092349218","display_name":"Hafize Merve Kestek","orcid":"https://orcid.org/0000-0002-9181-3554","observed_orcids":["https://orcid.org/0000-0002-9181-3554"]},"institutions":[{"id":"https://openalex.org/I137996928","display_name":"Sel\u00e7uk University","ror":"https://ror.org/045hgzm75","country_code":"TR","type":"education","lineage":["https://openalex.org/I137996928"]}],"countries":["TR"],"is_corresponding":false,"raw_author_name":"Hafize Merve Kestek","raw_affiliation_strings":["Sel\u00e7uk University, Faculty of Science, Department of Biochemistry, Konya, Turkey"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Sel\u00e7uk University, Faculty of Science, Department of Biochemistry, Konya, Turkey","institution_ids":["https://openalex.org/I137996928"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5036475318","display_name":"Murat T\u00fcrkteki","orcid":"https://orcid.org/0000-0001-5584-3572","observed_orcids":["https://orcid.org/0000-0001-5584-3572"]},"institutions":[{"id":"https://openalex.org/I169255954","display_name":"Bilecik \u015eeyh Edebali \u00dcniversitesi","ror":"https://ror.org/00dzfx204","country_code":"TR","type":"education","lineage":["https://openalex.org/I169255954"]}],"countries":["TR"],"is_corresponding":false,"raw_author_name":"Murat T\u00fcrkteki","raw_affiliation_strings":["Bilecik \u015eeyh Edebali University, Faculty of Humanities and Social Sciences, Department of Archaeology, Bilecik, Turkey"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Bilecik \u015eeyh Edebali University, Faculty of Humanities and Social Sciences, Department of Archaeology, Bilecik, Turkey","institution_ids":["https://openalex.org/I169255954"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":2,"corresponding_author_ids":["https://openalex.org/A5005689493"],"corresponding_institution_ids":["https://openalex.org/I137996928"],"apc_list":null,"apc_paid":null,"fwci":0.5448,"has_fulltext":true,"cited_by_count":1,"citation_normalized_percentile":{"value":0.73675565,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":{"min":91,"max":95},"biblio":{"volume":"78","issue":"9","first_page":"1231","last_page":"1243"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T10087","display_name":"Archaeology and ancient environmental studies","score":0.4950999915599823,"subfield":{"id":"https://openalex.org/subfields/3302","display_name":"Archeology"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},"topics":[{"id":"https://openalex.org/T10087","display_name":"Archaeology and ancient environmental studies","score":0.4950999915599823,"subfield":{"id":"https://openalex.org/subfields/3302","display_name":"Archeology"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},{"id":"https://openalex.org/T11212","display_name":"Cultural Heritage Materials Analysis","score":0.22010000050067902,"subfield":{"id":"https://openalex.org/subfields/1204","display_name":"Archeology (arts and humanities)"},"field":{"id":"https://openalex.org/fields/12","display_name":"Arts and Humanities"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},{"id":"https://openalex.org/T10909","display_name":"Edible Oils Quality and Analysis","score":0.09130000323057175,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/lipid-residues","display_name":"lipid residues","score":0.9070000052452087},{"id":"https://openalex.org/keywords/archaeological-ceramics","display_name":"archaeological ceramics","score":0.8289999961853027},{"id":"https://openalex.org/keywords/fatty-acid-composition","display_name":"fatty acid composition","score":0.7749999761581421},{"id":"https://openalex.org/keywords/silylation","display_name":"silylation","score":0.7670000195503235},{"id":"https://openalex.org/keywords/extraction-optimization","display_name":"extraction optimization","score":0.6729999780654907}],"concepts":[{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.7707746028900146},{"id":"https://openalex.org/C5304478","wikidata":"https://www.wikidata.org/wiki/Q502457","display_name":"Silylation","level":3,"score":0.6635869741439819},{"id":"https://openalex.org/C2781338088","wikidata":"https://www.wikidata.org/wiki/Q903495","display_name":"Residue (chemistry)","level":2,"score":0.6576477289199829},{"id":"https://openalex.org/C150077022","wikidata":"https://www.wikidata.org/wiki/Q3136137","display_name":"Response surface methodology","level":2,"score":0.6522071957588196},{"id":"https://openalex.org/C43617362","wikidata":"https://www.wikidata.org/wiki/Q170050","display_name":"Chromatography","level":1,"score":0.6494930982589722},{"id":"https://openalex.org/C134132462","wikidata":"https://www.wikidata.org/wiki/Q45621","display_name":"Ceramic","level":2,"score":0.6372904777526855},{"id":"https://openalex.org/C4725764","wikidata":"https://www.wikidata.org/wiki/Q844704","display_name":"Extraction (chemistry)","level":2,"score":0.6086410880088806},{"id":"https://openalex.org/C123460561","wikidata":"https://www.wikidata.org/wiki/Q677065","display_name":"Gas chromatography","level":2,"score":0.47155332565307617},{"id":"https://openalex.org/C162356407","wikidata":"https://www.wikidata.org/wiki/Q180809","display_name":"Mass spectrometry","level":2,"score":0.4358367919921875},{"id":"https://openalex.org/C161790260","wikidata":"https://www.wikidata.org/wiki/Q82264","display_name":"Catalysis","level":2,"score":0.253276526927948},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.16358304023742676}],"mesh":[],"locations_count":2,"locations":[{"id":"doi:10.1134/s1061934823090162","doi":"https://doi.org/10.1134/s1061934823090162","is_oa":false,"landing_page_url":"https://doi.org/10.1134/s1061934823090162","pdf_url":null,"source":{"id":"https://openalex.org/S3394804","display_name":"Journal of Analytical Chemistry","issn_l":"0021-8766","issn":["0021-8766","0044-4502","1061-9348","1608-3199","3034-512X"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-d","norway-1","poland-40","russia-white-list-1","russia-white-list-3","vabb-shw"],"host_organization":"https://openalex.org/P4310320267","host_organization_name":"Pleiades Publishing","host_organization_lineage":["https://openalex.org/P4310320267","https://openalex.org/P4310319965"],"host_organization_lineage_names":["Pleiades Publishing","Springer Nature"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Analytical Chemistry","raw_type":"journal-article"},{"id":"pmh:oai:acikkaynak.bilecik.edu.tr:11552/7607","doi":null,"is_oa":true,"landing_page_url":"https://hdl.handle.net/11552/7607","pdf_url":"https://acikkaynak.bilecik.edu.tr/bitstreams/d03e41c8-6e8d-402c-9ff0-89096d24aa59/download","source":{"id":"https://openalex.org/S7407055253","display_name":"Bilecik \u015eeyh Edebali University Institutional Repository","issn_l":null,"issn":null,"is_oa":false,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":null,"host_organization_name":null,"host_organization_lineage":[],"host_organization_lineage_names":[],"type":"repository"},"license":"cc-by-nc-nd","license_id":"https://openalex.org/licenses/cc-by-nc-nd","version":"submittedVersion","is_accepted":false,"is_published":false,"raw_source_name":null,"raw_type":"Article"}],"best_oa_location":{"id":"pmh:oai:acikkaynak.bilecik.edu.tr:11552/7607","doi":null,"is_oa":true,"landing_page_url":"https://hdl.handle.net/11552/7607","pdf_url":"https://acikkaynak.bilecik.edu.tr/bitstreams/d03e41c8-6e8d-402c-9ff0-89096d24aa59/download","source":{"id":"https://openalex.org/S7407055253","display_name":"Bilecik \u015eeyh Edebali University Institutional Repository","issn_l":null,"issn":null,"is_oa":false,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":null,"host_organization_name":null,"host_organization_lineage":[],"host_organization_lineage_names":[],"type":"repository"},"license":"cc-by-nc-nd","license_id":"https://openalex.org/licenses/cc-by-nc-nd","version":"submittedVersion","is_accepted":false,"is_published":false,"raw_source_name":null,"raw_type":"Article"},"sustainable_development_goals":[],"study_designs":[],"awards":[],"funders":[{"id":"https://openalex.org/F4320321656","display_name":"Ege \u00dcniversitesi","ror":"https://ror.org/02eaafc18"},{"id":"https://openalex.org/F4320324151","display_name":"Sel\u00e7uk \u00dcniversitesi","ror":"https://ror.org/045hgzm75"}],"has_content":{"grobid_xml":true,"pdf":true},"content_urls":{"pdf":"https://content.openalex.org/works/W4386700550.pdf","grobid_xml":"https://content.openalex.org/works/W4386700550.grobid-xml"},"referenced_works_count":47,"referenced_works":["https://openalex.org/W151488927","https://openalex.org/W192861976","https://openalex.org/W1608789804","https://openalex.org/W1655265300","https://openalex.org/W1726217820","https://openalex.org/W1979700785","https://openalex.org/W1983904247","https://openalex.org/W1986634900","https://openalex.org/W1991791093","https://openalex.org/W2006053877","https://openalex.org/W2007479279","https://openalex.org/W2008250667","https://openalex.org/W2012445058","https://openalex.org/W2054746384","https://openalex.org/W2060004594","https://openalex.org/W2061473410","https://openalex.org/W2070381250","https://openalex.org/W2070613772","https://openalex.org/W2078075407","https://openalex.org/W2080723191","https://openalex.org/W2083514735","https://openalex.org/W2089772683","https://openalex.org/W2102341368","https://openalex.org/W2108315807","https://openalex.org/W2128108320","https://openalex.org/W2135021848","https://openalex.org/W2157915669","https://openalex.org/W2166780575","https://openalex.org/W2171305706","https://openalex.org/W2254994036","https://openalex.org/W2302703048","https://openalex.org/W2304975092","https://openalex.org/W2340282906","https://openalex.org/W2347038360","https://openalex.org/W2499985755","https://openalex.org/W2519521223","https://openalex.org/W2564352017","https://openalex.org/W2600898016","https://openalex.org/W2780348949","https://openalex.org/W2909353576","https://openalex.org/W2940912281","https://openalex.org/W2951707740","https://openalex.org/W2971740365","https://openalex.org/W3040998477","https://openalex.org/W3135220945","https://openalex.org/W4213266667","https://openalex.org/W6912247502"],"related_works":["https://openalex.org/W2082769027","https://openalex.org/W7196982830","https://openalex.org/W1655265300","https://openalex.org/W6991001806","https://openalex.org/W7029352634","https://openalex.org/W7051640418","https://openalex.org/W2736703598","https://openalex.org/W7039508263","https://openalex.org/W3118795954","https://openalex.org/W2031526998"],"abstract_inverted_index":{"Abstract":[0],"In":[1],"this":[2,51],"study,":[3],"parameters":[4,138],"of":[5,16,31,119,139,175],"an":[6],"acid-catalyzed":[7],"direct":[8],"extraction":[9,141,156,174,197],"methylation":[10],"method":[11,82,142],"used":[12],"for":[13,172],"the":[14,21,47,60,64,80,90,100,111,115,129,137,140,146,151,155,166,173,176,180,184,193,196,205],"determination":[15],"low-level":[17],"lipid":[18,72,91,112,131,177],"residues":[19,92,113,178],"in":[20,46,94,114,179],"ceramic":[22,56,76,126,181],"artifacts":[23,57],"were":[24,69,83,96,143],"investigated":[25],"and":[26,89,122,136,158,169,183],"optimized":[27],"as":[28,163,165],"a":[29,188],"result":[30],"chemometric":[32,147],"modeling":[33],"techniques":[34],"that":[35,110],"enable":[36],"comprehensive":[37],"statistical":[38],"data":[39],"to":[40,71,99,150],"be":[41,108,161,201],"obtained":[42,101],"with":[43,128,198],"fewer":[44],"analyses":[45],"optimization":[48],"studies.":[49],"For":[50],"purpose,":[52],"25":[53],"amorphous":[54],"unglazed":[55],"found":[58],"during":[59],"1996\u20132021":[61],"excavations":[62],"at":[63],"K\u00fcll\u00fcoba":[65],"H\u00f6y\u00fck":[66],"archaeological":[67],"site":[68],"subjected":[70],"residue":[73,132],"determination.":[74],"The":[75,125],"samples":[77],"extracted":[78],"by":[79,85],"proposed":[81],"analyzed":[84,116],"gas":[86],"chromatography-mass":[87],"spectrometry,":[88],"present":[93],"them":[95],"determined.":[97],"According":[98,149],"fatty":[102],"acid":[103],"composition":[104],"results,":[105],"it":[106],"can":[107,200],"said":[109],"ceramics":[117],"are":[118],"both":[120],"animal":[121],"plant":[123],"origin.":[124],"artifact":[127],"highest":[130],"concentration":[133],"was":[134],"selected,":[135],"examined":[144],"using":[145],"models.":[148],"response":[152],"surface":[153],"methodology,":[154],"time":[157],"temperature":[159],"should":[160],"high":[162],"long":[164],"experimental":[167],"conditions":[168],"environment":[170],"allow":[171],"artifacts,":[182],"silylation":[185,206],"process":[186,207],"has":[187],"limited":[189],"positive":[190],"effect":[191],"on":[192],"yield,":[194],"but":[195],"methanol":[199],"achieved":[202],"successfully":[203],"when":[204],"is":[208],"not":[209],"performed.":[210]},"counts_by_year":[{"year":2026,"cited_by_count":1}],"updated_date":"2026-11-04T10:54:05.112534","created_date":"2023-09-14T00:00:00"}
