{"id":"https://openalex.org/W2156495087","doi":"https://doi.org/10.1039/ja9920700329","title":"Protocol for the design and interpretation of method evaluation in atomic absorption spectrometric analysis. Application to the determination of lead and manganese in blood","display_name":"Protocol for the design and interpretation of method evaluation in atomic absorption spectrometric analysis. Application to the determination of lead and manganese in blood","publication_year":1992,"publication_date":"1992-01-01","ids":{"openalex":"https://openalex.org/W2156495087","doi":"https://doi.org/10.1039/ja9920700329","mag":"2156495087"},"language":"en","primary_location":{"id":"doi:10.1039/ja9920700329","doi":"https://doi.org/10.1039/ja9920700329","is_oa":false,"landing_page_url":"https://doi.org/10.1039/ja9920700329","pdf_url":null,"source":{"id":"https://openalex.org/S26602194","display_name":"Journal of Analytical Atomic Spectrometry","issn_l":"0267-9477","issn":["0267-9477","1364-5544"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-d","jufo-1","norway-1","poland-100","russia-white-list-1","vabb-shw"],"host_organization":"https://openalex.org/P4310320556","host_organization_name":"Royal Society of Chemistry","host_organization_lineage":["https://openalex.org/P4310320556"],"host_organization_lineage_names":["Royal Society of Chemistry"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Analytical Atomic Spectrometry","raw_type":"journal-article"},"volume":null,"type":"article","indexed_in":["crossref"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5103282488","display_name":"Jan Christensen","orcid":"https://orcid.org/0000-0003-1114-7465","observed_orcids":["https://orcid.org/0000-0003-1114-7465"]},"institutions":[],"countries":[],"is_corresponding":false,"raw_author_name":"Jytte Molin Christensen","raw_affiliation_strings":[],"raw_orcid":null,"affiliations":[]},{"author_position":"middle","author":{"id":"https://openalex.org/A5054427789","display_name":"Otto Melchior Poulsen","orcid":"https://orcid.org/0000-0003-3127-9895","observed_orcids":["https://orcid.org/0000-0003-3127-9895"]},"institutions":[],"countries":[],"is_corresponding":false,"raw_author_name":"Otto Melchior Poulsen","raw_affiliation_strings":[],"raw_orcid":null,"affiliations":[]},{"author_position":"last","author":{"id":"https://openalex.org/A5036380080","display_name":"Thomas Anglov","orcid":null,"observed_orcids":[]},"institutions":[],"countries":[],"is_corresponding":false,"raw_author_name":"Thomas Anglov","raw_affiliation_strings":[],"raw_orcid":null,"affiliations":[]}],"institutions":[],"countries_distinct_count":0,"institutions_distinct_count":0,"corresponding_author_ids":[],"corresponding_institution_ids":[],"apc_list":null,"apc_paid":null,"fwci":4.7074,"has_fulltext":false,"cited_by_count":29,"citation_normalized_percentile":{"value":0.96487209,"is_in_top_1_percent":false,"is_in_top_10_percent":true},"cited_by_percentile_year":{"min":89,"max":95},"biblio":{"volume":"7","issue":"2","first_page":"329","last_page":"329"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T11890","display_name":"Scientific Measurement and Uncertainty Evaluation","score":0.9326000213623047,"subfield":{"id":"https://openalex.org/subfields/1804","display_name":"Statistics, Probability and Uncertainty"},"field":{"id":"https://openalex.org/fields/18","display_name":"Decision Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},"topics":[{"id":"https://openalex.org/T11890","display_name":"Scientific Measurement and Uncertainty Evaluation","score":0.9326000213623047,"subfield":{"id":"https://openalex.org/subfields/1804","display_name":"Statistics, Probability and Uncertainty"},"field":{"id":"https://openalex.org/fields/18","display_name":"Decision Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}},{"id":"https://openalex.org/T11314","display_name":"Clinical Laboratory Practices and Quality Control","score":0.030700000002980232,"subfield":{"id":"https://openalex.org/subfields/2737","display_name":"Physiology"},"field":{"id":"https://openalex.org/fields/27","display_name":"Medicine"},"domain":{"id":"https://openalex.org/domains/4","display_name":"Health Sciences"}},{"id":"https://openalex.org/T10180","display_name":"Analytical chemistry methods development","score":0.023499999195337296,"subfield":{"id":"https://openalex.org/subfields/1602","display_name":"Analytical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/method-evaluation","display_name":"method evaluation","score":0.921999990940094},{"id":"https://openalex.org/keywords/atomic-absorption-spectroscopy","display_name":"atomic absorption spectrometry","score":0.906000018119812},{"id":"https://openalex.org/keywords/blood-lead-levels","display_name":"blood lead levels","score":0.6959999799728394},{"id":"https://openalex.org/keywords/blood-manganese","display_name":"blood manganese","score":0.9710000157356262},{"id":"https://openalex.org/keywords/measurement-uncertainty","display_name":"measurement uncertainty","score":0.5979999899864197},{"id":"https://openalex.org/keywords/systematic-errors","display_name":"systematic errors","score":0.8489999771118164},{"id":"https://openalex.org/keywords/proportional-error","display_name":"proportional error","score":0.7770000100135803},{"id":"https://openalex.org/keywords/detection-limit","display_name":"detection limit","score":0.753000020980835},{"id":"https://openalex.org/keywords/limit-of-quantification","display_name":"limit of quantification","score":1.0},{"id":"https://openalex.org/keywords/statistical-control","display_name":"statistical control","score":0.6380000114440918},{"id":"https://openalex.org/keywords/quality-assurance","display_name":"quality assurance","score":0.621999979019165},{"id":"https://openalex.org/keywords/mean-squared-error","display_name":"mean squared error","score":0.6029999852180481}],"concepts":[{"id":"https://openalex.org/C139945424","wikidata":"https://www.wikidata.org/wiki/Q1940696","display_name":"Mean squared error","level":2,"score":0.6360690593719482},{"id":"https://openalex.org/C105795698","wikidata":"https://www.wikidata.org/wiki/Q12483","display_name":"Statistics","level":1,"score":0.5861932039260864},{"id":"https://openalex.org/C33619061","wikidata":"https://www.wikidata.org/wiki/Q655346","display_name":"Atomic absorption spectroscopy","level":2,"score":0.5455722808837891},{"id":"https://openalex.org/C122383733","wikidata":"https://www.wikidata.org/wiki/Q865920","display_name":"Approximation error","level":2,"score":0.4823872148990631},{"id":"https://openalex.org/C22679943","wikidata":"https://www.wikidata.org/wiki/Q159375","display_name":"Standard deviation","level":2,"score":0.4662071168422699},{"id":"https://openalex.org/C18747219","wikidata":"https://www.wikidata.org/wiki/Q620994","display_name":"Standard error","level":2,"score":0.453289270401001},{"id":"https://openalex.org/C123614077","wikidata":"https://www.wikidata.org/wiki/Q1364905","display_name":"Propagation of uncertainty","level":2,"score":0.4140239953994751},{"id":"https://openalex.org/C33923547","wikidata":"https://www.wikidata.org/wiki/Q395","display_name":"Mathematics","level":0,"score":0.40569913387298584},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.40196746587753296},{"id":"https://openalex.org/C113196181","wikidata":"https://www.wikidata.org/wiki/Q485223","display_name":"Analytical Chemistry (journal)","level":2,"score":0.36053940653800964},{"id":"https://openalex.org/C43617362","wikidata":"https://www.wikidata.org/wiki/Q170050","display_name":"Chromatography","level":1,"score":0.13681307435035706},{"id":"https://openalex.org/C121332964","wikidata":"https://www.wikidata.org/wiki/Q413","display_name":"Physics","level":0,"score":0.10003331303596497},{"id":"https://openalex.org/C62520636","wikidata":"https://www.wikidata.org/wiki/Q944","display_name":"Quantum mechanics","level":1,"score":0.0}],"mesh":[],"locations_count":1,"locations":[{"id":"doi:10.1039/ja9920700329","doi":"https://doi.org/10.1039/ja9920700329","is_oa":false,"landing_page_url":"https://doi.org/10.1039/ja9920700329","pdf_url":null,"source":{"id":"https://openalex.org/S26602194","display_name":"Journal of Analytical Atomic Spectrometry","issn_l":"0267-9477","issn":["0267-9477","1364-5544"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-d","jufo-1","norway-1","poland-100","russia-white-list-1","vabb-shw"],"host_organization":"https://openalex.org/P4310320556","host_organization_name":"Royal Society of Chemistry","host_organization_lineage":["https://openalex.org/P4310320556"],"host_organization_lineage_names":["Royal Society of Chemistry"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Analytical Atomic Spectrometry","raw_type":"journal-article"}],"best_oa_location":null,"sustainable_development_goals":[],"study_designs":[],"awards":[],"funders":[],"has_content":{"pdf":false,"grobid_xml":false},"content_urls":null,"referenced_works_count":4,"referenced_works":["https://openalex.org/W1965460767","https://openalex.org/W2002206916","https://openalex.org/W2068795164","https://openalex.org/W2085214931"],"related_works":["https://openalex.org/W2005365355","https://openalex.org/W2378367567","https://openalex.org/W2901865122","https://openalex.org/W7096982593","https://openalex.org/W2144758315","https://openalex.org/W4244380656","https://openalex.org/W2369361562","https://openalex.org/W2364584918","https://openalex.org/W2357332255","https://openalex.org/W2351829732"],"abstract_inverted_index":{"Results":[0],"of":[1,6,33,42,58,99,106,109,123,142,145,151,156,160,169,187,205,214,226,247,254,271,286,290,296,300,328],"measurements":[2],"should":[3,15],"be":[4,315],"independent":[5],"the":[7,10,13,18,38,76,84,93,100,107,110,113,117,124,128,136,143,146,149,154,161,166,170,176,180,184,188,194,203,206,211,215,224,245,255,269,283,326],"laboratory":[8,14],"performing":[9],"analysis.":[11],"Hence":[12,183],"document":[16],"that":[17],"method":[19,43,67,77,114,137,216,233],"retains":[20],"statistical":[21,52,80],"control,":[22,81],"is":[23,78,103,120],"without":[24],"systematic":[25,147,177,199],"errors":[26],"and":[27,40,60,130,153,165,210,260,264,277,292,307,324],"has":[28],"an":[29,104],"acceptably":[30],"low":[31],"level":[32],"uncertainty.":[34,182],"A":[35],"protocol":[36],"for":[37,219,258,318,325],"design":[39,69,116,139,313],"interpretation":[41],"evaluation":[44,68,115,138,217],"in":[45,62,79,223,321,332],"atomic":[46],"absorption":[47],"spectrometry":[48],"(AAS)":[49],"using":[50],"ordinary":[51],"calculations":[53],"was":[54,234,302],"applied":[55],"to":[56,88,244],"determinations":[57],"lead":[59,232,261],"manganese":[61,259],"blood":[63,231],"by":[64],"AAS.":[65],"The":[66,96,158,198,230,251,298,312],"provides":[70],"information":[71],"on":[72],"whether":[73,83],"or":[74],"not":[75],"i.e.,":[82,126],"values":[85],"observed":[86],"belong":[87],"a":[89,248],"normal":[90,101],"distribution":[91,102],"around":[92],"mean":[94,162,172,190],"values.":[95],"standard":[97],"deviation":[98],"expression":[105],"uncertainty":[108,119,253],"method.":[111],"Using":[112],"estimated":[118,201],"truly":[121],"representative":[122],"methods,":[125],"both":[127],"within-run":[129],"between-run":[131],"variations":[132],"are":[133],"included.":[134],"Further,":[135],"produces":[140],"estimates":[141],"magnitude":[144,204],"error,":[148,200],"limit":[150,155,270,299],"detection":[152,272],"quantification.":[157],"application":[159],"square":[163,167,173,185,191],"error":[164,174,178,192,209,213],"root":[168,186],"relative":[171,189],"combines":[175],"with":[179],"total":[181,195],"depicts":[193],"analytical":[196,256,329],"error.":[197,250],"as":[202],"zero":[207],"point":[208],"proportional":[212,249],"functions":[218],"Zeeman-effect":[220],"AAS":[221,322],"methods":[222,257],"determination":[225],"manganese,":[227],"were":[228,262],"negligible.":[229],"unacceptable":[235],"at":[236,282],"concentrations":[237],"higher":[238],"than":[239],"200":[240],"\u00b5g":[241,266,275,280,288,294,305,310],"dm\u20133":[242,276,281,289,295,306],"owing":[243],"presence":[246],"combined":[252],"1.00":[263],"11.1":[265],"dm\u20133,":[267],"respectively,":[268],"LODMn=":[273],"0.2":[274],"LODPb=":[278],"12":[279],"concentration":[284],"levels":[285],"11":[287],"Mn":[291],"72":[293],"Pb.":[297],"quantification":[301],"LOQMn=":[303],"2.8":[304],"LOQPb=":[308],"33.7":[309],"dm\u20133.":[311],"can":[314],"conveniently":[316],"used":[317],"quality":[319],"assurance":[320],"analysis":[323],"characterization":[327],"chemical":[330],"methodology":[331],"general.":[333]},"counts_by_year":[{"year":2023,"cited_by_count":2},{"year":2022,"cited_by_count":1},{"year":2018,"cited_by_count":1},{"year":2016,"cited_by_count":1},{"year":2013,"cited_by_count":1}],"updated_date":"2025-11-06T03:46:38.306776","created_date":"2016-06-24T00:00:00"}
