{"id":"https://openalex.org/W2008239181","doi":"https://doi.org/10.1021/la990514f","title":"Microemulsion-Mediated Hydrothermal Synthesis and Characterization of Nanosize Rutile and Anatase Particles","display_name":"Microemulsion-Mediated Hydrothermal Synthesis and Characterization of Nanosize Rutile and Anatase Particles","publication_year":1999,"publication_date":"1999-11-11","ids":{"openalex":"https://openalex.org/W2008239181","doi":"https://doi.org/10.1021/la990514f","mag":"2008239181"},"language":"en","primary_location":{"id":"doi:10.1021/la990514f","doi":"https://doi.org/10.1021/la990514f","is_oa":false,"landing_page_url":"https://doi.org/10.1021/la990514f","pdf_url":null,"source":{"id":"https://openalex.org/S75741262","display_name":"Langmuir","issn_l":"0743-7463","issn":["0743-7463","1520-5827"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-d","doyens","jufo-2","ki-jl-1","medline","norway-1","poland-100","russia-white-list-1","vabb-shw"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Langmuir","raw_type":"journal-article"},"parent_works":[],"lineage":["https://openalex.org/W2008239181"],"child_works_count":0,"type":"article","is_traditional":true,"indexed_in":["crossref"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5083511365","display_name":"Mingmei M. Wu","orcid":"https://orcid.org/0000-0001-8087-3925","observed_orcids":["https://orcid.org/0000-0001-8087-3925"]},"institutions":[{"id":"https://openalex.org/I4391768096","display_name":"State Key Laboratory of Inorganic Synthesis and Preparative Chemistry","ror":"https://ror.org/03ed91q10","country_code":"CN","type":"facility","lineage":["https://openalex.org/I194450716","https://openalex.org/I4391768096"]}],"countries":["CN"],"is_corresponding":false,"raw_author_name":"Mingmei Wu","raw_affiliation_strings":["Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","institution_ids":["https://openalex.org/I4391768096"]},{"raw_affiliation_string":"School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China","institution_ids":[]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5009081336","display_name":"Junbiao Long","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I4391768096","display_name":"State Key Laboratory of Inorganic Synthesis and Preparative Chemistry","ror":"https://ror.org/03ed91q10","country_code":"CN","type":"facility","lineage":["https://openalex.org/I194450716","https://openalex.org/I4391768096"]}],"countries":["CN"],"is_corresponding":false,"raw_author_name":"Junbiao Long","raw_affiliation_strings":["Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","institution_ids":["https://openalex.org/I4391768096"]},{"raw_affiliation_string":"School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China","institution_ids":[]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5028084165","display_name":"Aihong Huang","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I4391768096","display_name":"State Key Laboratory of Inorganic Synthesis and Preparative Chemistry","ror":"https://ror.org/03ed91q10","country_code":"CN","type":"facility","lineage":["https://openalex.org/I194450716","https://openalex.org/I4391768096"]}],"countries":["CN"],"is_corresponding":false,"raw_author_name":"Aihong Huang","raw_affiliation_strings":["Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","institution_ids":["https://openalex.org/I4391768096"]},{"raw_affiliation_string":"School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China","institution_ids":[]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5103434083","display_name":"Yuji Luo","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I4391768096","display_name":"State Key Laboratory of Inorganic Synthesis and Preparative Chemistry","ror":"https://ror.org/03ed91q10","country_code":"CN","type":"facility","lineage":["https://openalex.org/I194450716","https://openalex.org/I4391768096"]}],"countries":["CN"],"is_corresponding":false,"raw_author_name":"Yuji Luo","raw_affiliation_strings":["Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","institution_ids":["https://openalex.org/I4391768096"]},{"raw_affiliation_string":"School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China","institution_ids":[]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5101519300","display_name":"Shouhua Feng","orcid":"https://orcid.org/0000-0001-6888-068X","observed_orcids":["https://orcid.org/0000-0001-6888-068X","https://orcid.org/0000-0002-1070-1148","https://orcid.org/0000-0002-6967-0155"]},"institutions":[{"id":"https://openalex.org/I4391768096","display_name":"State Key Laboratory of Inorganic Synthesis and Preparative Chemistry","ror":"https://ror.org/03ed91q10","country_code":"CN","type":"facility","lineage":["https://openalex.org/I194450716","https://openalex.org/I4391768096"]}],"countries":["CN"],"is_corresponding":false,"raw_author_name":"Shouhua Feng","raw_affiliation_strings":["Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","institution_ids":["https://openalex.org/I4391768096"]},{"raw_affiliation_string":"School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China","institution_ids":[]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5074028379","display_name":"Ruren Xu","orcid":"https://orcid.org/0000-0001-5406-6951","observed_orcids":["https://orcid.org/0000-0001-5406-6951"]},"institutions":[{"id":"https://openalex.org/I4391768096","display_name":"State Key Laboratory of Inorganic Synthesis and Preparative Chemistry","ror":"https://ror.org/03ed91q10","country_code":"CN","type":"facility","lineage":["https://openalex.org/I194450716","https://openalex.org/I4391768096"]}],"countries":["CN"],"is_corresponding":false,"raw_author_name":"Ruren Xu","raw_affiliation_strings":["Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Changchun 130022, P. R. China","institution_ids":["https://openalex.org/I4391768096"]},{"raw_affiliation_string":"School of Chemistry and Chemical Engineering, Zhongshan University, Guangzhou 510275, P. R. China","institution_ids":[]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":[],"corresponding_institution_ids":["https://openalex.org/I4391768096"],"apc_list":{"value":4500,"currency":"USD","value_usd":4500},"apc_paid":null,"fwci":4.5654,"has_fulltext":false,"cited_by_count":175,"citation_normalized_percentile":{"value":0.92830189,"is_in_top_1_percent":false,"is_in_top_10_percent":true},"cited_by_percentile_year":{"min":87,"max":99},"biblio":{"volume":"15","issue":"26","first_page":"8822","last_page":"8825"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T10024","display_name":"TiO2 Photocatalysis and Solar Cells","score":0.7724999785423279,"subfield":{"id":"https://openalex.org/subfields/2105","display_name":"Renewable Energy, Sustainability and the Environment"},"field":{"id":"https://openalex.org/fields/21","display_name":"Energy"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T10024","display_name":"TiO2 Photocatalysis and Solar Cells","score":0.7724999785423279,"subfield":{"id":"https://openalex.org/subfields/2105","display_name":"Renewable Energy, Sustainability and the Environment"},"field":{"id":"https://openalex.org/fields/21","display_name":"Energy"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10721","display_name":"Surfactants and Colloidal Systems","score":0.0794999971985817,"subfield":{"id":"https://openalex.org/subfields/1606","display_name":"Physical and Theoretical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10735","display_name":"Mesoporous Materials and Catalysis","score":0.07500000298023224,"subfield":{"id":"https://openalex.org/subfields/2505","display_name":"Materials Chemistry"},"field":{"id":"https://openalex.org/fields/25","display_name":"Materials Science"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/rutile-nanoparticles","display_name":"rutile nanoparticles","score":0.8019999861717224},{"id":"https://openalex.org/keywords/anatase-nanoparticles","display_name":"anatase nanoparticles","score":0.9990000128746033},{"id":"https://openalex.org/keywords/titanium-dioxide","display_name":"titanium dioxide","score":0.6700000166893005},{"id":"https://openalex.org/keywords/microemulsions","display_name":"microemulsions","score":0.5680000185966492},{"id":"https://openalex.org/keywords/triton-x-100","display_name":"Triton X-100","score":0.8510000109672546},{"id":"https://openalex.org/keywords/tetrabutyl-titanate","display_name":"tetrabutyl titanate","score":0.9269999861717224},{"id":"https://openalex.org/keywords/particle-morphology","display_name":"particle morphology","score":0.6389999985694885},{"id":"https://openalex.org/keywords/grain-size","display_name":"grain size","score":0.6859999895095825},{"id":"https://openalex.org/keywords/reaction-conditions","display_name":"reaction conditions","score":0.5329999923706055}],"concepts":[{"id":"https://openalex.org/C190119865","wikidata":"https://www.wikidata.org/wiki/Q338019","display_name":"Microemulsion","level":3,"score":0.9627660512924194},{"id":"https://openalex.org/C2777402863","wikidata":"https://www.wikidata.org/wiki/Q413357","display_name":"Anatase","level":4,"score":0.654578685760498},{"id":"https://openalex.org/C156622251","wikidata":"https://www.wikidata.org/wiki/Q1036221","display_name":"Hydrothermal circulation","level":2,"score":0.6052947044372559},{"id":"https://openalex.org/C42360764","wikidata":"https://www.wikidata.org/wiki/Q83588","display_name":"Chemical engineering","level":1,"score":0.5823604464530945},{"id":"https://openalex.org/C155672457","wikidata":"https://www.wikidata.org/wiki/Q61231","display_name":"Nanoparticle","level":2,"score":0.5726040005683899},{"id":"https://openalex.org/C2778237882","wikidata":"https://www.wikidata.org/wiki/Q211433","display_name":"Cyclohexane","level":2,"score":0.5631168484687805},{"id":"https://openalex.org/C192562407","wikidata":"https://www.wikidata.org/wiki/Q228736","display_name":"Materials science","level":0,"score":0.5617516040802002},{"id":"https://openalex.org/C2776871784","wikidata":"https://www.wikidata.org/wiki/Q10861356","display_name":"Hydrothermal synthesis","level":3,"score":0.5307671427726746},{"id":"https://openalex.org/C7082614","wikidata":"https://www.wikidata.org/wiki/Q849523","display_name":"Calcination","level":3,"score":0.5006685256958008},{"id":"https://openalex.org/C184651966","wikidata":"https://www.wikidata.org/wiki/Q906356","display_name":"Aqueous solution","level":2,"score":0.46883124113082886},{"id":"https://openalex.org/C179104552","wikidata":"https://www.wikidata.org/wiki/Q11165","display_name":"Inorganic chemistry","level":1,"score":0.4551614820957184},{"id":"https://openalex.org/C2777889555","wikidata":"https://www.wikidata.org/wiki/Q320603","display_name":"Rutile","level":2,"score":0.4148569703102112},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.3541125953197479},{"id":"https://openalex.org/C58226133","wikidata":"https://www.wikidata.org/wiki/Q1324199","display_name":"Pulmonary surfactant","level":2,"score":0.2350921332836151},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.22593256831169128},{"id":"https://openalex.org/C171250308","wikidata":"https://www.wikidata.org/wiki/Q11468","display_name":"Nanotechnology","level":1,"score":0.2036806344985962},{"id":"https://openalex.org/C161790260","wikidata":"https://www.wikidata.org/wiki/Q82264","display_name":"Catalysis","level":2,"score":0.15129530429840088},{"id":"https://openalex.org/C65165184","wikidata":"https://www.wikidata.org/wiki/Q218831","display_name":"Photocatalysis","level":3,"score":0.08195832371711731},{"id":"https://openalex.org/C127413603","wikidata":"https://www.wikidata.org/wiki/Q11023","display_name":"Engineering","level":0,"score":0.0}],"mesh":[],"locations_count":1,"locations":[{"id":"doi:10.1021/la990514f","doi":"https://doi.org/10.1021/la990514f","is_oa":false,"landing_page_url":"https://doi.org/10.1021/la990514f","pdf_url":null,"source":{"id":"https://openalex.org/S75741262","display_name":"Langmuir","issn_l":"0743-7463","issn":["0743-7463","1520-5827"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-d","doyens","jufo-2","ki-jl-1","medline","norway-1","poland-100","russia-white-list-1","vabb-shw"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Langmuir","raw_type":"journal-article"}],"best_oa_location":null,"sustainable_development_goals":[],"study_designs":[],"awards":[],"funders":[],"has_content":{"pdf":false,"grobid_xml":false},"content_urls":null,"referenced_works_count":27,"referenced_works":["https://openalex.org/W1968179359","https://openalex.org/W1973872260","https://openalex.org/W1973884850","https://openalex.org/W1979407338","https://openalex.org/W1980738929","https://openalex.org/W1984185978","https://openalex.org/W1984407878","https://openalex.org/W1985385783","https://openalex.org/W1985621016","https://openalex.org/W1986959589","https://openalex.org/W1991101882","https://openalex.org/W2003379154","https://openalex.org/W2029899647","https://openalex.org/W2035176265","https://openalex.org/W2050862450","https://openalex.org/W2057556367","https://openalex.org/W2060393563","https://openalex.org/W2080018786","https://openalex.org/W2091551345","https://openalex.org/W2094288727","https://openalex.org/W2114827914","https://openalex.org/W2126822973","https://openalex.org/W2129381909","https://openalex.org/W2146392479","https://openalex.org/W2168524298","https://openalex.org/W2951090698","https://openalex.org/W2951896472"],"related_works":["https://openalex.org/W2155666735","https://openalex.org/W2486123725","https://openalex.org/W2072875570","https://openalex.org/W2023949634","https://openalex.org/W2014523734","https://openalex.org/W2012942562","https://openalex.org/W2011808610","https://openalex.org/W2002400097","https://openalex.org/W2032925518","https://openalex.org/W2951896472"],"abstract_inverted_index":{"Uniform":[0],"nanoparticles":[1,38],"of":[2,31,56,74,83,109,116,129,137,155,171,175,183,187,201],"rutile":[3],"and":[4,33,97,142,149,152,163,199],"anatase":[5],"were":[6,120,157],"prepared,":[7],"respectively,":[8],"by":[9,24,87,159,164],"a":[10,13,43,81,126],"new":[11],"approach,":[12],"microemulsion-mediated":[14,44,69],"method,":[15],"in":[16,71,102],"which":[17,72],"the":[18,28,54,66,98,107,110,150,173,176,181,185,189,193,197,202],"microemulsion":[19,32,111],"medium":[20],"was":[21,76,85,100,140],"further":[22],"treated":[23],"hydrothermal":[25,34,45,133,138],"reaction.":[26],"Herein,":[27],"combined":[29],"procedure":[30],"synthesis":[35,139],"to":[36,41,53],"prepare":[37],"is":[39],"referred":[40],"as":[42,122,180],"(MMH)":[46],"method.":[47],"This":[48],"MMH":[49],"method":[50],"could":[51],"lead":[52],"formation":[55],"crystalline":[57],"titania":[58,130,203],"powders":[59],"under":[60,132],"much":[61],"milder":[62],"reaction":[63,177,190,194],"conditions":[64],"than":[65],"normally":[67],"reported":[68],"methods,":[70],"posttreatment":[73],"calcination":[75],"necessary.":[77],"In":[78],"this":[79],"work,":[80],"kind":[82],"solution":[84,99],"formed":[86],"dissolving":[88],"tetrabutyl":[89],"titanate":[90],"into":[91],"hydrochloric":[92],"acid":[93],"or":[94],"nitric":[95],"acid,":[96,184,188],"dispersed":[101],"an":[103],"organic":[104],"phase":[105,147],"for":[106,125,144],"preparation":[108],"medium.":[112],"The":[113,135,146,169],"aqueous":[114],"cores":[115],"water/Triton":[117],"X-100/hexanol/cyclohexane":[118],"microemulsions":[119],"used":[121],"constrained":[123],"microreactors":[124],"controlled":[127],"growth":[128],"particles":[131],"conditions.":[134],"product":[136,204],"separated":[141],"dried":[143],"characterization.":[145],"components":[148],"morphologies":[151,200],"grain":[153],"sizes":[154],"products":[156],"determined":[158],"X-ray":[160],"diffraction":[161],"(XRD)":[162],"transmission":[165],"electron":[166],"microscopy":[167],"(TEM).":[168],"effects":[170],"changing":[172],"variables":[174],"conditions,":[178],"such":[179],"use":[182],"concentrations":[186],"temperatures,":[191],"and/or":[192],"times":[195],"on":[196],"phases":[198],"are":[205],"described.":[206]},"counts_by_year":[{"year":2026,"cited_by_count":1},{"year":2025,"cited_by_count":1},{"year":2024,"cited_by_count":1},{"year":2023,"cited_by_count":1},{"year":2022,"cited_by_count":2},{"year":2021,"cited_by_count":4},{"year":2020,"cited_by_count":4},{"year":2019,"cited_by_count":4},{"year":2018,"cited_by_count":5},{"year":2017,"cited_by_count":3},{"year":2016,"cited_by_count":4},{"year":2015,"cited_by_count":7},{"year":2014,"cited_by_count":13},{"year":2013,"cited_by_count":11},{"year":2012,"cited_by_count":13}],"updated_date":"2026-11-12T12:28:57.059296","created_date":"2016-06-24T00:00:00"}