{"id":"https://openalex.org/W2007369811","doi":"https://doi.org/10.1021/ac0262513","title":"Microwave-Assisted Steam Distillation for Simple Determination of Polychlorinated Biphenyls and Organochlorine Pesticides in Sediments","display_name":"Microwave-Assisted Steam Distillation for Simple Determination of Polychlorinated Biphenyls and Organochlorine Pesticides in Sediments","publication_year":2003,"publication_date":"2003-02-13","ids":{"openalex":"https://openalex.org/W2007369811","doi":"https://doi.org/10.1021/ac0262513","mag":"2007369811","pmid":"https://pubmed.ncbi.nlm.nih.gov/12659209"},"language":"en","primary_location":{"id":"doi:10.1021/ac0262513","doi":"https://doi.org/10.1021/ac0262513","is_oa":false,"landing_page_url":"https://doi.org/10.1021/ac0262513","pdf_url":null,"source":{"id":"https://openalex.org/S191963794","display_name":"Analytical Chemistry","issn_l":"0003-2700","issn":["0003-2700","1520-6882"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-class-a","anvur-scientific","cwts-core","dongbi-a","doyens","jufo-3","ki-jl-2","medline","norway-2","poland-140","russia-white-list-1","vabb-shw"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Analytical Chemistry","raw_type":"journal-article"},"volume":null,"type":"article","is_traditional":true,"indexed_in":["crossref","pubmed"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5050624941","display_name":"Masahiko Numata","orcid":"https://orcid.org/0000-0003-4660-9682","observed_orcids":["https://orcid.org/0000-0003-4660-9682"]},"institutions":[{"id":"https://openalex.org/I4405273829","display_name":"National Metrology Institute of Japan","ror":"https://ror.org/00j3eeb74","country_code":"JP","type":"government","lineage":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]},{"id":"https://openalex.org/I73613424","display_name":"National Institute of Advanced Industrial Science and Technology","ror":"https://ror.org/01703db54","country_code":"JP","type":"government","lineage":["https://openalex.org/I73613424"]}],"countries":["JP"],"is_corresponding":true,"raw_author_name":"Masahiko Numata","raw_affiliation_strings":["National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan","institution_ids":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5020079920","display_name":"Takashi Yarita","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I4405273829","display_name":"National Metrology Institute of Japan","ror":"https://ror.org/00j3eeb74","country_code":"JP","type":"government","lineage":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]},{"id":"https://openalex.org/I73613424","display_name":"National Institute of Advanced Industrial Science and Technology","ror":"https://ror.org/01703db54","country_code":"JP","type":"government","lineage":["https://openalex.org/I73613424"]}],"countries":["JP"],"is_corresponding":false,"raw_author_name":"Takashi Yarita","raw_affiliation_strings":["National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan","institution_ids":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5089040037","display_name":"Yoshie Aoyagi","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I4405273829","display_name":"National Metrology Institute of Japan","ror":"https://ror.org/00j3eeb74","country_code":"JP","type":"government","lineage":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]},{"id":"https://openalex.org/I73613424","display_name":"National Institute of Advanced Industrial Science and Technology","ror":"https://ror.org/01703db54","country_code":"JP","type":"government","lineage":["https://openalex.org/I73613424"]}],"countries":["JP"],"is_corresponding":false,"raw_author_name":"Yoshie Aoyagi","raw_affiliation_strings":["National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan","institution_ids":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5068339342","display_name":"Akiko Takatsu","orcid":"https://orcid.org/0000-0002-5689-8812","observed_orcids":["https://orcid.org/0000-0002-5689-8812"]},"institutions":[{"id":"https://openalex.org/I4405273829","display_name":"National Metrology Institute of Japan","ror":"https://ror.org/00j3eeb74","country_code":"JP","type":"government","lineage":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]},{"id":"https://openalex.org/I73613424","display_name":"National Institute of Advanced Industrial Science and Technology","ror":"https://ror.org/01703db54","country_code":"JP","type":"government","lineage":["https://openalex.org/I73613424"]}],"countries":["JP"],"is_corresponding":false,"raw_author_name":"Akiko Takatsu","raw_affiliation_strings":["National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"National Metrology Institute of Japan, AIST, Tsukuba, Ibaraki 305-8563, Japan","institution_ids":["https://openalex.org/I4405273829","https://openalex.org/I73613424"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":2,"corresponding_author_ids":["https://openalex.org/A5050624941"],"corresponding_institution_ids":["https://openalex.org/I4405273829","https://openalex.org/I73613424"],"apc_list":{"value":4500,"currency":"USD","value_usd":4500},"apc_paid":null,"fwci":4.446,"has_fulltext":false,"cited_by_count":37,"citation_normalized_percentile":{"value":0.95114077,"is_in_top_1_percent":false,"is_in_top_10_percent":true},"cited_by_percentile_year":{"min":88,"max":96},"biblio":{"volume":"75","issue":"6","first_page":"1450","last_page":"1457"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T10180","display_name":"Analytical chemistry methods development","score":0.6937999725341797,"subfield":{"id":"https://openalex.org/subfields/1602","display_name":"Analytical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T10180","display_name":"Analytical chemistry methods development","score":0.6937999725341797,"subfield":{"id":"https://openalex.org/subfields/1602","display_name":"Analytical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10122","display_name":"Toxic Organic Pollutants Impact","score":0.18410000205039978,"subfield":{"id":"https://openalex.org/subfields/2307","display_name":"Health, Toxicology and Mutagenesis"},"field":{"id":"https://openalex.org/fields/23","display_name":"Environmental Science"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T11423","display_name":"Pesticide Residue Analysis and Safety","score":0.08569999784231186,"subfield":{"id":"https://openalex.org/subfields/1106","display_name":"Food Science"},"field":{"id":"https://openalex.org/fields/11","display_name":"Agricultural and Biological Sciences"},"domain":{"id":"https://openalex.org/domains/1","display_name":"Life Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/microwave-assisted-extraction","display_name":"microwave-assisted extraction","score":0.9520000219345093},{"id":"https://openalex.org/keywords/polychlorinated-biphenyls","display_name":"polychlorinated biphenyls","score":0.9980000257492065},{"id":"https://openalex.org/keywords/organochlorine-pesticides","display_name":"organochlorine pesticides","score":1.0},{"id":"https://openalex.org/keywords/marine-sediments","display_name":"marine sediment","score":0.8489999771118164},{"id":"https://openalex.org/keywords/sample-extraction","display_name":"sample extraction","score":0.7369999885559082},{"id":"https://openalex.org/keywords/water-vapor-desorption","display_name":"water vapor desorption","score":0.6579999923706055},{"id":"https://openalex.org/keywords/soxhlet-extraction","display_name":"Soxhlet extraction","score":0.7059999704360962},{"id":"https://openalex.org/keywords/lindane","display_name":"lindane","score":0.6790000200271606},{"id":"https://openalex.org/keywords/p-p-dde","display_name":"p,p'-DDE","score":0.8550000190734863},{"id":"https://openalex.org/keywords/isotope-labeled-internal-standards","display_name":"isotope-labeled internal standards","score":0.7639999985694885},{"id":"https://openalex.org/keywords/extraction-recovery","display_name":"extraction recovery","score":0.5690000057220459}],"concepts":[{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.8349459171295166},{"id":"https://openalex.org/C63663721","wikidata":"https://www.wikidata.org/wiki/Q1164392","display_name":"Steam distillation","level":3,"score":0.7315130233764648},{"id":"https://openalex.org/C43617362","wikidata":"https://www.wikidata.org/wiki/Q170050","display_name":"Chromatography","level":1,"score":0.6444323062896729},{"id":"https://openalex.org/C4725764","wikidata":"https://www.wikidata.org/wiki/Q844704","display_name":"Extraction (chemistry)","level":2,"score":0.6280810832977295},{"id":"https://openalex.org/C107872376","wikidata":"https://www.wikidata.org/wiki/Q321355","display_name":"Environmental chemistry","level":1,"score":0.6011049747467041},{"id":"https://openalex.org/C100859065","wikidata":"https://www.wikidata.org/wiki/Q906323","display_name":"Certified reference materials","level":3,"score":0.5407976508140564},{"id":"https://openalex.org/C123460561","wikidata":"https://www.wikidata.org/wiki/Q677065","display_name":"Gas chromatography","level":2,"score":0.5375912189483643},{"id":"https://openalex.org/C2778576202","wikidata":"https://www.wikidata.org/wiki/Q2540164","display_name":"Sample preparation","level":2,"score":0.516167938709259},{"id":"https://openalex.org/C204030448","wikidata":"https://www.wikidata.org/wiki/Q101017","display_name":"Distillation","level":2,"score":0.5143412351608276},{"id":"https://openalex.org/C2779423988","wikidata":"https://www.wikidata.org/wiki/Q409682","display_name":"Hexachlorobenzene","level":3,"score":0.4774516224861145},{"id":"https://openalex.org/C2776275140","wikidata":"https://www.wikidata.org/wiki/Q127956","display_name":"Microwave oven","level":3,"score":0.46006786823272705},{"id":"https://openalex.org/C10390740","wikidata":"https://www.wikidata.org/wiki/Q2282401","display_name":"Analyte","level":2,"score":0.43368467688560486},{"id":"https://openalex.org/C2780471494","wikidata":"https://www.wikidata.org/wiki/Q146505","display_name":"Solvent","level":2,"score":0.41070619225502014},{"id":"https://openalex.org/C44838205","wikidata":"https://www.wikidata.org/wiki/Q127995","display_name":"Microwave","level":2,"score":0.2956358790397644},{"id":"https://openalex.org/C82685317","wikidata":"https://www.wikidata.org/wiki/Q19829510","display_name":"Pollutant","level":2,"score":0.1539667248725891},{"id":"https://openalex.org/C119128265","wikidata":"https://www.wikidata.org/wiki/Q900165","display_name":"Detection limit","level":2,"score":0.1404218077659607},{"id":"https://openalex.org/C121332964","wikidata":"https://www.wikidata.org/wiki/Q413","display_name":"Physics","level":0,"score":0.0},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.0},{"id":"https://openalex.org/C62520636","wikidata":"https://www.wikidata.org/wiki/Q944","display_name":"Quantum mechanics","level":1,"score":0.0}],"mesh":[{"descriptor_ui":"D007306","descriptor_name":"Insecticides","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":true},{"descriptor_ui":"D008401","descriptor_name":"Gas Chromatography-Mass Spectrometry","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D008872","descriptor_name":"Microwaves","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D011078","descriptor_name":"Polychlorinated Biphenyls","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":true},{"descriptor_ui":"D012997","descriptor_name":"Solvents","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D013227","descriptor_name":"Steam","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D019015","descriptor_name":"Geologic Sediments","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":false}],"locations_count":2,"locations":[{"id":"doi:10.1021/ac0262513","doi":"https://doi.org/10.1021/ac0262513","is_oa":false,"landing_page_url":"https://doi.org/10.1021/ac0262513","pdf_url":null,"source":{"id":"https://openalex.org/S191963794","display_name":"Analytical Chemistry","issn_l":"0003-2700","issn":["0003-2700","1520-6882"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-class-a","anvur-scientific","cwts-core","dongbi-a","doyens","jufo-3","ki-jl-2","medline","norway-2","poland-140","russia-white-list-1","vabb-shw"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Analytical Chemistry","raw_type":"journal-article"},{"id":"pmid:12659209","doi":null,"is_oa":false,"landing_page_url":"https://pubmed.ncbi.nlm.nih.gov/12659209","pdf_url":null,"source":{"id":"https://openalex.org/S4306525036","display_name":"PubMed","issn_l":null,"issn":null,"is_oa":false,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":"https://openalex.org/I1299303238","host_organization_name":"National Institutes of Health","host_organization_lineage":["https://openalex.org/I1299303238"],"host_organization_lineage_names":[],"type":"repository"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Analytical chemistry","raw_type":"Journal Article"}],"best_oa_location":null,"sustainable_development_goals":[],"study_designs":[],"awards":[],"funders":[],"has_content":{"grobid_xml":false,"pdf":false},"content_urls":null,"referenced_works_count":19,"referenced_works":["https://openalex.org/W1974397759","https://openalex.org/W1975326112","https://openalex.org/W1987913630","https://openalex.org/W1990848788","https://openalex.org/W1991333647","https://openalex.org/W1998082650","https://openalex.org/W2010353842","https://openalex.org/W2011283231","https://openalex.org/W2016901584","https://openalex.org/W2029806680","https://openalex.org/W2046481429","https://openalex.org/W2057505994","https://openalex.org/W2057795813","https://openalex.org/W2061933584","https://openalex.org/W2063580167","https://openalex.org/W2076299022","https://openalex.org/W2087166750","https://openalex.org/W2102351464","https://openalex.org/W4300647633"],"related_works":["https://openalex.org/W1991222481","https://openalex.org/W2073142405","https://openalex.org/W2409617322","https://openalex.org/W1523096719","https://openalex.org/W2045264810","https://openalex.org/W2078763132","https://openalex.org/W1530230949","https://openalex.org/W2013685981","https://openalex.org/W2036100693","https://openalex.org/W2074782257"],"abstract_inverted_index":{"A":[0,49],"novel":[1],"sample":[2,50,60],"extraction":[3,23,56,151,219],"technique":[4,148,209],"for":[5,68,206],"polychlorinated":[6],"biphenyls":[7,176],"(PCBs)":[8],"and":[9,25,111,132,149,157,160,180,221],"organochlorine":[10],"pesticides":[11],"(OCPs)":[12],"analysis":[13],"using":[14,142],"microwave-heating":[15],"device":[16],"is":[17],"developed.":[18],"In":[19],"this":[20,143,168],"study,":[21],"microwave-assisted":[22,144],"(MAE)":[24],"steam":[26,145,154],"distillation":[27,146],"techniques":[28],"were":[29,79,139,186],"combined.":[30],"Desorption":[31],"of":[32,84,128,162,173,201],"the":[33,59,65,72,90,163,207,214,222,226],"anatytes":[34],"from":[35,61,125],"solid":[36],"matrixes":[37],"was":[38,44],"accelerated":[39],"with":[40,64,81,96,190,213],"water":[41],"vapor":[42],"which":[43],"generated":[45],"by":[46,141,217],"microwave":[47,55],"irradiation.":[48],"holder":[51],"in":[52,117,167,225],"a":[53,126,133],"commercial":[54],"cell":[57],"kept":[58],"direct":[62],"contact":[63],"organic":[66],"solvent":[67],"analytes":[69,192],"trapping":[70],"during":[71],"treatment":[73],"process.":[74],"Therefore,":[75],"relatively":[76,181],"clean":[77],"extracts":[78],"obtained":[80,91,216],"small":[82],"amount":[83],"solvents.":[85],"Without":[86],"any":[87],"cleanup":[88],"steps,":[89],"extract":[92],"could":[93],"be":[94],"analyzed":[95,140],"gas":[97],"chromatograph/mass":[98],"spectrometers":[99],"(GC/MS).":[100],"Six":[101],"PCB":[102],"congeners":[103],"(PCB15,":[104,193],"28,":[105,194],"70,":[106,195],"101,":[107,196],"180,":[108],"194,":[109,178],"209)":[110,179],"three":[112],"OCPs":[113,183],"(gamma-HCH,":[114,184],"4,4'-DDE,":[115],"4,4'-DDD)":[116,185],"two":[118],"marine":[119],"sediment":[120,123],"samples":[121],"(a":[122],"collected":[124],"bay":[127],"Kyusyu":[129],"Island,":[130],"Japan,":[131],"certified":[134,223],"reference":[135],"material":[136],"NIST":[137],"SRM1944)":[138],"(MASD)":[147],"another":[150],"method":[152],"(exhaustive":[153],"distillation,":[155],"MAE,":[156],"Soxhlet":[158],"extraction);":[159],"comparisons":[161],"results":[164,212],"are":[165],"shown":[166],"report.":[169],"Although":[170],"recovery":[171],"yields":[172],"highly":[174],"chlorinated":[175],"(PCB180,":[177],"polar":[182],"low":[187],"(30-60%)":[188],"compared":[189],"other":[191,218],"4,4'-DDE;":[197],"recovery,":[198],"80-100%),":[199],"use":[200],"isotope":[202],"labeled":[203],"internal":[204],"standards":[205],"MASD":[208],"gave":[210],"comparable":[211],"values":[215,224],"methods":[220],"samples.":[227]},"counts_by_year":[{"year":2025,"cited_by_count":1},{"year":2024,"cited_by_count":1},{"year":2020,"cited_by_count":1},{"year":2018,"cited_by_count":1},{"year":2016,"cited_by_count":2},{"year":2015,"cited_by_count":1},{"year":2013,"cited_by_count":1},{"year":2012,"cited_by_count":2}],"updated_date":"2026-10-31T12:09:11.096373","created_date":"2016-06-24T00:00:00"}
