{"id":"https://openalex.org/W1982499693","doi":"https://doi.org/10.1021/ed2004774","title":"Solid-State NMR Spectroscopy for the Physical Chemistry Laboratory","display_name":"Solid-State NMR Spectroscopy for the Physical Chemistry Laboratory","publication_year":2012,"publication_date":"2012-12-14","ids":{"openalex":"https://openalex.org/W1982499693","doi":"https://doi.org/10.1021/ed2004774","mag":"1982499693"},"language":"en","primary_location":{"id":"doi:10.1021/ed2004774","doi":"https://doi.org/10.1021/ed2004774","is_oa":false,"landing_page_url":"https://doi.org/10.1021/ed2004774","pdf_url":null,"source":{"id":"https://openalex.org/S105208853","display_name":"Journal of Chemical Education","issn_l":"0021-9584","issn":["0021-9584","1938-1328"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-c","erih-plus","jufo-1","ki-jl-1","norway-1","poland-70","russia-white-list-1"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Chemical Education","raw_type":"journal-article"},"volume":null,"type":"article","indexed_in":["crossref"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5087962253","display_name":"Jacob J. Kinnun","orcid":"https://orcid.org/0000-0002-2579-1553","observed_orcids":["https://orcid.org/0000-0002-2579-1553"]},"institutions":[{"id":"https://openalex.org/I138006243","display_name":"University of Arizona","ror":"https://ror.org/03m2x1q45","country_code":"US","type":"education","lineage":["https://openalex.org/I138006243"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Jacob J. Kinnun","raw_affiliation_strings":["Department of Physics and \u2021Department of Chemistry and Biochemistry, University of Arizona, Tucson, Arizona\r85721, United States"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Department of Physics and \u2021Department of Chemistry and Biochemistry, University of Arizona, Tucson, Arizona\r85721, United States","institution_ids":["https://openalex.org/I138006243"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5090597319","display_name":"Avigdor Leftin","orcid":"https://orcid.org/0000-0002-4560-8162","observed_orcids":["https://orcid.org/0000-0002-4560-8162"]},"institutions":[{"id":"https://openalex.org/I138006243","display_name":"University of Arizona","ror":"https://ror.org/03m2x1q45","country_code":"US","type":"education","lineage":["https://openalex.org/I138006243"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Avigdor Leftin","raw_affiliation_strings":["Department of Physics and \u2021Department of Chemistry and Biochemistry, University of Arizona, Tucson, Arizona\r85721, United States"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Department of Physics and \u2021Department of Chemistry and Biochemistry, University of Arizona, Tucson, Arizona\r85721, United States","institution_ids":["https://openalex.org/I138006243"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5005781724","display_name":"Michael F. Brown","orcid":"https://orcid.org/0000-0003-4154-0241","observed_orcids":["https://orcid.org/0000-0003-4154-0241"]},"institutions":[{"id":"https://openalex.org/I138006243","display_name":"University of Arizona","ror":"https://ror.org/03m2x1q45","country_code":"US","type":"education","lineage":["https://openalex.org/I138006243"]}],"countries":["US"],"is_corresponding":true,"raw_author_name":"Michael F. Brown","raw_affiliation_strings":["Department of Physics and \u2021Department of Chemistry and Biochemistry, University of Arizona, Tucson, Arizona\r85721, United States"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Department of Physics and \u2021Department of Chemistry and Biochemistry, University of Arizona, Tucson, Arizona\r85721, United States","institution_ids":["https://openalex.org/I138006243"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":["https://openalex.org/A5005781724"],"corresponding_institution_ids":["https://openalex.org/I138006243"],"apc_list":{"value":4500,"currency":"USD","value_usd":4500},"apc_paid":null,"fwci":0.5643,"has_fulltext":false,"cited_by_count":32,"citation_normalized_percentile":{"value":0.57126327,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":{"min":89,"max":98},"biblio":{"volume":"90","issue":"1","first_page":"123","last_page":"128"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T11809","display_name":"Advanced NMR Techniques and Applications","score":0.6714000105857849,"subfield":{"id":"https://openalex.org/subfields/1607","display_name":"Spectroscopy"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T11809","display_name":"Advanced NMR Techniques and Applications","score":0.6714000105857849,"subfield":{"id":"https://openalex.org/subfields/1607","display_name":"Spectroscopy"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T12327","display_name":"Various Chemistry Research Topics","score":0.31150001287460327,"subfield":{"id":"https://openalex.org/subfields/1606","display_name":"Physical and Theoretical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T14097","display_name":"Chemistry Education and Research","score":0.002400000113993883,"subfield":{"id":"https://openalex.org/subfields/3304","display_name":"Education"},"field":{"id":"https://openalex.org/fields/33","display_name":"Social Sciences"},"domain":{"id":"https://openalex.org/domains/2","display_name":"Social Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/solid-state-nmr","display_name":"solid-state NMR","score":0.9490000009536743},{"id":"https://openalex.org/keywords/deuterium-nmr","display_name":"deuterium NMR","score":0.9070000052452087},{"id":"https://openalex.org/keywords/hexamethylbenzene","display_name":"hexamethylbenzene","score":0.8690000176429749},{"id":"https://openalex.org/keywords/methyl-group-rotation","display_name":"methyl group rotation","score":0.6859999895095825},{"id":"https://openalex.org/keywords/molecular-mobility","display_name":"molecular mobility","score":0.6629999876022339},{"id":"https://openalex.org/keywords/quantum-mechanics","display_name":"quantum mechanics","score":0.531000018119812}],"concepts":[{"id":"https://openalex.org/C2776513212","wikidata":"https://www.wikidata.org/wiki/Q413592","display_name":"Hexamethylbenzene","level":3,"score":0.7960571050643921},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.7308805584907532},{"id":"https://openalex.org/C153202636","wikidata":"https://www.wikidata.org/wiki/Q7557802","display_name":"Solid-state nuclear magnetic resonance","level":2,"score":0.6792346239089966},{"id":"https://openalex.org/C66974803","wikidata":"https://www.wikidata.org/wiki/Q10359898","display_name":"Nuclear magnetic resonance spectroscopy","level":2,"score":0.5914692878723145},{"id":"https://openalex.org/C67020732","wikidata":"https://www.wikidata.org/wiki/Q7068131","display_name":"Nuclear magnetic resonance crystallography","level":4,"score":0.5206034183502197},{"id":"https://openalex.org/C32891209","wikidata":"https://www.wikidata.org/wiki/Q483666","display_name":"Spectroscopy","level":2,"score":0.4836519956588745},{"id":"https://openalex.org/C100705429","wikidata":"https://www.wikidata.org/wiki/Q5037892","display_name":"Carbon-13 NMR satellite","level":4,"score":0.48030561208724976},{"id":"https://openalex.org/C116447816","wikidata":"https://www.wikidata.org/wiki/Q3415253","display_name":"Fluorine-19 NMR","level":3,"score":0.4791145324707031},{"id":"https://openalex.org/C67787023","wikidata":"https://www.wikidata.org/wiki/Q6954755","display_name":"NMR spectra database","level":3,"score":0.4633859097957611},{"id":"https://openalex.org/C46141821","wikidata":"https://www.wikidata.org/wiki/Q209402","display_name":"Nuclear magnetic resonance","level":1,"score":0.3718445301055908},{"id":"https://openalex.org/C159467904","wikidata":"https://www.wikidata.org/wiki/Q2001702","display_name":"Chemical physics","level":1,"score":0.37106698751449585},{"id":"https://openalex.org/C113196181","wikidata":"https://www.wikidata.org/wiki/Q485223","display_name":"Analytical Chemistry (journal)","level":2,"score":0.3561927080154419},{"id":"https://openalex.org/C147597530","wikidata":"https://www.wikidata.org/wiki/Q369472","display_name":"Computational chemistry","level":1,"score":0.3379051685333252},{"id":"https://openalex.org/C4839761","wikidata":"https://www.wikidata.org/wiki/Q212111","display_name":"Spectral line","level":2,"score":0.32116925716400146},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.21063321828842163},{"id":"https://openalex.org/C121332964","wikidata":"https://www.wikidata.org/wiki/Q413","display_name":"Physics","level":0,"score":0.13257119059562683},{"id":"https://openalex.org/C2777691172","wikidata":"https://www.wikidata.org/wiki/Q2270","display_name":"Benzene","level":2,"score":0.0},{"id":"https://openalex.org/C1276947","wikidata":"https://www.wikidata.org/wiki/Q333","display_name":"Astronomy","level":1,"score":0.0},{"id":"https://openalex.org/C62520636","wikidata":"https://www.wikidata.org/wiki/Q944","display_name":"Quantum mechanics","level":1,"score":0.0}],"mesh":[],"locations_count":1,"locations":[{"id":"doi:10.1021/ed2004774","doi":"https://doi.org/10.1021/ed2004774","is_oa":false,"landing_page_url":"https://doi.org/10.1021/ed2004774","pdf_url":null,"source":{"id":"https://openalex.org/S105208853","display_name":"Journal of Chemical Education","issn_l":"0021-9584","issn":["0021-9584","1938-1328"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-c","erih-plus","jufo-1","ki-jl-1","norway-1","poland-70","russia-white-list-1"],"host_organization":"https://openalex.org/P4310320006","host_organization_name":"American Chemical Society","host_organization_lineage":["https://openalex.org/P4310320006"],"host_organization_lineage_names":["American Chemical Society"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of Chemical Education","raw_type":"journal-article"}],"best_oa_location":null,"sustainable_development_goals":[],"sustainable_development_goals_aurora":[],"study_designs":[],"awards":[],"funders":[],"has_content":{"grobid_xml":false,"pdf":false},"content_urls":null,"referenced_works_count":11,"referenced_works":["https://openalex.org/W585276791","https://openalex.org/W590701767","https://openalex.org/W600590637","https://openalex.org/W1565564534","https://openalex.org/W2018622350","https://openalex.org/W2033681820","https://openalex.org/W2058561930","https://openalex.org/W2061529631","https://openalex.org/W2095359460","https://openalex.org/W2151924302","https://openalex.org/W2496268021"],"related_works":["https://openalex.org/W2989839185","https://openalex.org/W7062008298","https://openalex.org/W6958549802","https://openalex.org/W608699634","https://openalex.org/W2017853040","https://openalex.org/W2245557429","https://openalex.org/W64041536","https://openalex.org/W225004003","https://openalex.org/W1969292233","https://openalex.org/W3185400266"],"abstract_inverted_index":{"Solid-state":[0],"nuclear":[1,140],"magnetic":[2],"resonance":[3],"(NMR)":[4],"spectroscopy":[5,41],"finds":[6],"growing":[7],"application":[8],"to":[9,108,111,138,194],"inorganic":[10],"and":[11,18,42,79,162,239],"organic":[12],"materials,":[13],"biological":[14],"samples,":[15],"polymers,":[16],"proteins,":[17],"cellular":[19],"membranes.":[20],"However,":[21],"this":[22,170],"technique":[23],"is":[24,72,106],"often":[25],"neither":[26],"included":[27],"in":[28,34,46,61,74,98,145,150,204,221,242],"laboratory":[29],"curricula":[30],"nor":[31],"typically":[32],"covered":[33],"undergraduate":[35,48,100,183,208],"courses.":[36],"On":[37],"the":[38,53,76,81,109,113,139,151,159,166,243],"other":[39],"hand,":[40],"molecular":[43,148,180,230],"structure":[44],"taught":[45],"second-semester":[47],"physical":[49,222],"chemistry":[50,223],"courses":[51],"meet":[52],"minimal":[54],"background":[55],"prerequisites":[56],"for":[57],"interpreting":[58],"data":[59],"obtained":[60],"many":[62,99,207],"solid-state":[63,67,186],"NMR":[64,70,94,116,189],"experiments.":[65],"A":[66,102],"2":[68,114,187],"H":[69,115,188],"experiment":[71],"described":[73],"which":[75],"student":[77],"obtains":[78],"interprets":[80],"spectrum":[82,119],"of":[83,87,120,127,147,158,165,216,229,235],"a":[84,92,121,213],"powder":[85,124],"sample":[86,110,125],"hexamethylbenzene-":[88],"d":[89],"18":[90],"using":[91,199],"solution":[93],"spectrometer":[95],"as":[96,219,225,227,233],"found":[97],"institutions.":[101,209],"quadrupolar-echo":[103],"pulse":[104],"sequence":[105],"applied":[107],"obtain":[112],"spectrum.":[117],"The":[118,134],"randomly":[122],"oriented":[123],"consists":[126],"two":[128],"spectral":[129],"branches":[130],"with":[131],"broad":[132],"shoulders.":[133],"quadrupolar":[135],"frequencies":[136],"corresponding":[137],"spin":[141],"transitions":[142],"are":[143,202],"interpreted":[144],"terms":[146],"mobility":[149],"solid":[152,175,244],"state,":[153],"that":[154,174,201],"is,":[155],"3-fold":[156],"rotation":[157,164,234],"methyl":[160,240],"groups":[161,241],"6-fold":[163],"hexamethylbenzene":[167],"ring.":[168],"In":[169],"way,":[171],"students":[172],"discover":[173],"substances":[176],"may":[177],"have":[178],"significant":[179],"motions.":[181],"This":[182],"investigation":[184],"employing":[185],"provides":[190],"an":[191],"informative":[192],"exposure":[193],"state-of-the-art":[195],"research":[196],"techniques":[197],"by":[198],"facilities":[200],"already":[203],"place":[205],"at":[206],"Furthermore,":[210],"it":[211],"demonstrates":[212],"real-life":[214],"manifestation":[215],"quantum":[217],"mechanics":[218],"explained":[220],"courses,":[224],"well":[226],"fundamentals":[228],"motions":[231],"such":[232],"aromatic":[236],"ring":[237],"compounds":[238],"state.":[245]},"counts_by_year":[{"year":2026,"cited_by_count":2},{"year":2025,"cited_by_count":4},{"year":2024,"cited_by_count":1},{"year":2023,"cited_by_count":2},{"year":2022,"cited_by_count":4},{"year":2021,"cited_by_count":4},{"year":2020,"cited_by_count":1},{"year":2019,"cited_by_count":3},{"year":2018,"cited_by_count":2},{"year":2017,"cited_by_count":3},{"year":2016,"cited_by_count":2},{"year":2015,"cited_by_count":1},{"year":2014,"cited_by_count":3}],"updated_date":"2026-10-12T09:40:04.860316","created_date":"2016-06-24T00:00:00"}