{"id":"https://openalex.org/W1961659255","doi":"https://doi.org/10.1002/0471264229.os082.23","title":"Preparation of [1\u2010(Methoxymethylcarbamoyl)ethyl] Phosphonic Acid Bis\u2010(2,2,2\u2010trifluoroethyl) Ester: A Useful Intermediate in the Synthesis of Z \u2010Unsaturated N \u2010Methoxy\u2010 N \u2010Methylamides","display_name":"Preparation of [1\u2010(Methoxymethylcarbamoyl)ethyl] Phosphonic Acid Bis\u2010(2,2,2\u2010trifluoroethyl) Ester: A Useful Intermediate in the Synthesis of Z \u2010Unsaturated N \u2010Methoxy\u2010 N \u2010Methylamides","publication_year":2005,"publication_date":"2005-10-10","ids":{"openalex":"https://openalex.org/W1961659255","doi":"https://doi.org/10.1002/0471264229.os082.23","mag":"1961659255"},"language":"en","primary_location":{"id":"doi:10.1002/0471264229.os082.23","doi":"https://doi.org/10.1002/0471264229.os082.23","is_oa":false,"landing_page_url":"https://doi.org/10.1002/0471264229.os082.23","pdf_url":null,"source":{"id":"https://openalex.org/S101014958","display_name":"Organic Syntheses","issn_l":"0078-6209","issn":["0078-6209","2333-3553"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-c","jufo-1","norway-1","poland-20","russia-white-list-3"],"host_organization":"https://openalex.org/P4310320595","host_organization_name":"Wiley","host_organization_lineage":["https://openalex.org/P4310320595"],"host_organization_lineage_names":["Wiley"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Organic Syntheses","raw_type":"other"},"volume":{"id":"https://openalex.org/W4233591321","display_name":"Organic Syntheses"},"type":"other","indexed_in":["crossref"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5066527875","display_name":"Amos B. Smith","orcid":"https://orcid.org/0000-0002-1712-8567","observed_orcids":["https://orcid.org/0000-0002-1712-8567"]},"institutions":[{"id":"https://openalex.org/I79576946","display_name":"University of Pennsylvania","ror":"https://ror.org/00b30xv10","country_code":"US","type":"education","lineage":["https://openalex.org/I79576946"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Amos B. Smith","raw_affiliation_strings":["University of Pennsylvania, Department of Chemistry, Philadelphia"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"University of Pennsylvania, Department of Chemistry, Philadelphia","institution_ids":["https://openalex.org/I79576946"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5012643385","display_name":"Jason J. Beiger","orcid":"https://orcid.org/0000-0002-3073-0499","observed_orcids":["https://orcid.org/0000-0002-3073-0499"]},"institutions":[{"id":"https://openalex.org/I79576946","display_name":"University of Pennsylvania","ror":"https://ror.org/00b30xv10","country_code":"US","type":"education","lineage":["https://openalex.org/I79576946"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Jason J. Beiger","raw_affiliation_strings":["University of Pennsylvania, Department of Chemistry, Philadelphia"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"University of Pennsylvania, Department of Chemistry, Philadelphia","institution_ids":["https://openalex.org/I79576946"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5091579995","display_name":"Akin H. Davulcu","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I79576946","display_name":"University of Pennsylvania","ror":"https://ror.org/00b30xv10","country_code":"US","type":"education","lineage":["https://openalex.org/I79576946"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Akin H. Davulcu","raw_affiliation_strings":["University of Pennsylvania, Department of Chemistry, Philadelphia"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"University of Pennsylvania, Department of Chemistry, Philadelphia","institution_ids":["https://openalex.org/I79576946"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5103035478","display_name":"Jason M. Cox","orcid":"https://orcid.org/0000-0002-6247-9155","observed_orcids":["https://orcid.org/0000-0002-6247-9155"]},"institutions":[{"id":"https://openalex.org/I79576946","display_name":"University of Pennsylvania","ror":"https://ror.org/00b30xv10","country_code":"US","type":"education","lineage":["https://openalex.org/I79576946"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Jason M. Cox","raw_affiliation_strings":["University of Pennsylvania, Department of Chemistry, Philadelphia, PA 19104","University of Pennsylvania, Department of Chemistry, Philadelphia"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"University of Pennsylvania, Department of Chemistry, Philadelphia, PA 19104","institution_ids":["https://openalex.org/I79576946"]},{"raw_affiliation_string":"University of Pennsylvania, Department of Chemistry, Philadelphia","institution_ids":["https://openalex.org/I79576946"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":[],"corresponding_institution_ids":["https://openalex.org/I79576946"],"apc_list":null,"apc_paid":null,"fwci":null,"has_fulltext":false,"cited_by_count":2,"citation_normalized_percentile":null,"cited_by_percentile_year":null,"biblio":{"volume":null,"issue":null,"first_page":"147","last_page":"156"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T11748","display_name":"Organophosphorus compounds synthesis","score":0.9922000169754028,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},"topics":[{"id":"https://openalex.org/T11748","display_name":"Organophosphorus compounds synthesis","score":0.9922000169754028,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T13239","display_name":"Phosphorus compounds and reactions","score":0.005499999970197678,"subfield":{"id":"https://openalex.org/subfields/1605","display_name":"Organic Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10947","display_name":"Fluorine in Organic Chemistry","score":0.00039999998989515007,"subfield":{"id":"https://openalex.org/subfields/3003","display_name":"Pharmaceutical Science"},"field":{"id":"https://openalex.org/fields/30","display_name":"Pharmacology, Toxicology and Pharmaceutics"},"domain":{"id":"https://openalex.org/domains/1","display_name":"Life Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/hexamethyldisilazane","display_name":"hexamethyldisilazane","score":0.8550000190734863},{"id":"https://openalex.org/keywords/n-butyllithium","display_name":"n-butyllithium","score":0.7350000143051147},{"id":"https://openalex.org/keywords/organofluorine-synthesis","display_name":"organofluorine synthesis","score":0.5720000267028809}],"concepts":[{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.9371383190155029},{"id":"https://openalex.org/C2779607525","wikidata":"https://www.wikidata.org/wiki/Q14982","display_name":"Methanol","level":2,"score":0.6947261691093445},{"id":"https://openalex.org/C2780161600","wikidata":"https://www.wikidata.org/wiki/Q153","display_name":"Ethanol","level":2,"score":0.6813947558403015},{"id":"https://openalex.org/C2776460385","wikidata":"https://www.wikidata.org/wiki/Q420060","display_name":"Hydrochloride","level":2,"score":0.6273911595344543},{"id":"https://openalex.org/C2994242795","wikidata":"https://www.wikidata.org/wiki/Q101487","display_name":"Ethyl ester","level":2,"score":0.6189563274383545},{"id":"https://openalex.org/C2779485729","wikidata":"https://www.wikidata.org/wiki/Q210385","display_name":"Pyridine","level":2,"score":0.5695685744285583},{"id":"https://openalex.org/C2778541603","wikidata":"https://www.wikidata.org/wiki/Q152763","display_name":"Lithium (medication)","level":2,"score":0.5616233944892883},{"id":"https://openalex.org/C2778695967","wikidata":"https://www.wikidata.org/wiki/Q44791900","display_name":"Chloride","level":2,"score":0.5054507255554199},{"id":"https://openalex.org/C155647269","wikidata":"https://www.wikidata.org/wiki/Q243455","display_name":"Medicinal chemistry","level":1,"score":0.4846249520778656},{"id":"https://openalex.org/C2777241282","wikidata":"https://www.wikidata.org/wiki/Q591576","display_name":"Transesterification","level":3,"score":0.4745795726776123},{"id":"https://openalex.org/C178790620","wikidata":"https://www.wikidata.org/wiki/Q11351","display_name":"Organic chemistry","level":1,"score":0.4307732582092285},{"id":"https://openalex.org/C2781066024","wikidata":"https://www.wikidata.org/wiki/Q156","display_name":"Alcohol","level":2,"score":0.42983928322792053},{"id":"https://openalex.org/C134018914","wikidata":"https://www.wikidata.org/wiki/Q162606","display_name":"Endocrinology","level":1,"score":0.0},{"id":"https://openalex.org/C71924100","wikidata":"https://www.wikidata.org/wiki/Q11190","display_name":"Medicine","level":0,"score":0.0}],"mesh":[],"locations_count":1,"locations":[{"id":"doi:10.1002/0471264229.os082.23","doi":"https://doi.org/10.1002/0471264229.os082.23","is_oa":false,"landing_page_url":"https://doi.org/10.1002/0471264229.os082.23","pdf_url":null,"source":{"id":"https://openalex.org/S101014958","display_name":"Organic Syntheses","issn_l":"0078-6209","issn":["0078-6209","2333-3553"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["cwts-core","dongbi-c","jufo-1","norway-1","poland-20","russia-white-list-3"],"host_organization":"https://openalex.org/P4310320595","host_organization_name":"Wiley","host_organization_lineage":["https://openalex.org/P4310320595"],"host_organization_lineage_names":["Wiley"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Organic Syntheses","raw_type":"other"}],"best_oa_location":null,"sustainable_development_goals":[],"study_designs":[],"awards":[],"funders":[],"has_content":{"pdf":false,"grobid_xml":false},"content_urls":null,"referenced_works_count":10,"referenced_works":["https://openalex.org/W1964732329","https://openalex.org/W1981038207","https://openalex.org/W2024186923","https://openalex.org/W2030785805","https://openalex.org/W2042937679","https://openalex.org/W2094871139","https://openalex.org/W2120959935","https://openalex.org/W2144872179","https://openalex.org/W2950649638","https://openalex.org/W2953378992"],"related_works":["https://openalex.org/W2952425135","https://openalex.org/W2031000655","https://openalex.org/W1909761435","https://openalex.org/W2400739272","https://openalex.org/W1987391751","https://openalex.org/W1986838643","https://openalex.org/W2272001022","https://openalex.org/W1544809165","https://openalex.org/W761885047","https://openalex.org/W2214038634"],"abstract_inverted_index":{"Abstract":[0],"n":[1],"\u2010Butyl":[2],"lithium":[3],"Ethanamine,":[4],"N":[5,7,17,23,25],",":[6,8],"\u2010diethyl":[9],"Ethanol,":[10],"2,2,2\u2010trifluoro\u2010":[11],"Ethylphosphonic":[12],"acid":[13,29],"bis\u2010(2,2,2\u2010trifluoroethyl)ester":[14],"1,1,1,3,3,3,\u2010Hexamethyldisilazane":[15],"Methanamine,":[16],"\u2010methoxy\u2010,":[18],"hydrochloride":[19],"Methanol,":[20],"trichloro\u2010,":[21],"carbonate":[22],"\u2010Methoxy\u2010":[24],"\u2010methylcarbamoyl":[26],"chloride":[27],"[1\u2010(Methoxymethylcarbamoyl)ethyl]phosphonic":[28],"bis\u2010(2,2,2\u2010trifluoroethyl)":[30],"ester":[31],"Phosphonic":[32],"dichloride":[33],"Pyridine":[34]},"counts_by_year":[{"year":2019,"cited_by_count":1},{"year":2016,"cited_by_count":1}],"updated_date":"2026-10-10T09:11:00.788812","created_date":"2016-06-24T00:00:00"}