{"id":"https://openalex.org/W194874780","doi":"https://doi.org/10.1093/jaoac/94.3.931","title":"Analysis of Pesticides Residues in Fresh Produce Using Buffered Acetonitrile Extraction and Aminopropyl Cleanup with Gas Chromatography/Triple Quadrupole Mass Spectrometry, Liquid Chromatography/Triple Quadrupole Mass Spectrometry, Gas Chromatography/Ion Trap Detector Mass Spectrometry, and GC with a Halogen-Specific Detector","display_name":"Analysis of Pesticides Residues in Fresh Produce Using Buffered Acetonitrile Extraction and Aminopropyl Cleanup with Gas Chromatography/Triple Quadrupole Mass Spectrometry, Liquid Chromatography/Triple Quadrupole Mass Spectrometry, Gas Chromatography/Ion Trap Detector Mass Spectrometry, and GC with a Halogen-Specific Detector","publication_year":2011,"publication_date":"2011-05-01","ids":{"openalex":"https://openalex.org/W194874780","doi":"https://doi.org/10.1093/jaoac/94.3.931","mag":"194874780","pmid":"https://pubmed.ncbi.nlm.nih.gov/21797022"},"language":"en","primary_location":{"id":"doi:10.1093/jaoac/94.3.931","doi":"https://doi.org/10.1093/jaoac/94.3.931","is_oa":false,"landing_page_url":"https://doi.org/10.1093/jaoac/94.3.931","pdf_url":null,"source":{"id":"https://openalex.org/S103486911","display_name":"Journal of AOAC International","issn_l":"1060-3271","issn":["1060-3271","1944-7922"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-b","jufo-1","medline","norway-1","poland-40","russia-white-list-2","vabb-shw"],"host_organization":"https://openalex.org/P4310311648","host_organization_name":"Oxford University Press","host_organization_lineage":["https://openalex.org/P4310311648","https://openalex.org/P4310311647"],"host_organization_lineage_names":["Oxford University Press","University of Oxford"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC INTERNATIONAL","raw_type":"journal-article"},"volume":null,"type":"article","is_traditional":true,"indexed_in":["crossref","pubmed"],"open_access":{"is_oa":false,"oa_status":"closed","oa_url":null,"any_repository_has_fulltext":false},"authorships":[{"author_position":"first","author":{"id":"https://openalex.org/A5030016724","display_name":"Amy N Brown","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I1308724467","display_name":"Florida Department of Agriculture and Consumer Services","ror":"https://ror.org/058nbms57","country_code":"US","type":"government","lineage":["https://openalex.org/I1308724467"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Amy N Brown","raw_affiliation_strings":["Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650, USA"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","institution_ids":["https://openalex.org/I1308724467"]},{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650, USA","institution_ids":["https://openalex.org/I1308724467"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5075985200","display_name":"Jo Marie Cook","orcid":"https://orcid.org/0000-0002-7319-1253","observed_orcids":["https://orcid.org/0000-0002-7319-1253"]},"institutions":[{"id":"https://openalex.org/I1308724467","display_name":"Florida Department of Agriculture and Consumer Services","ror":"https://ror.org/058nbms57","country_code":"US","type":"government","lineage":["https://openalex.org/I1308724467"]}],"countries":["US"],"is_corresponding":true,"raw_author_name":"Jo Marie Cook","raw_affiliation_strings":["Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","institution_ids":["https://openalex.org/I1308724467"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5087727407","display_name":"Walter Hammack","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I1308724467","display_name":"Florida Department of Agriculture and Consumer Services","ror":"https://ror.org/058nbms57","country_code":"US","type":"government","lineage":["https://openalex.org/I1308724467"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Walter T Hammack","raw_affiliation_strings":["Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","institution_ids":["https://openalex.org/I1308724467"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5005323563","display_name":"Jason S Stepp","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I1308724467","display_name":"Florida Department of Agriculture and Consumer Services","ror":"https://ror.org/058nbms57","country_code":"US","type":"government","lineage":["https://openalex.org/I1308724467"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Jason S Stepp","raw_affiliation_strings":["Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","institution_ids":["https://openalex.org/I1308724467"]}]},{"author_position":"middle","author":{"id":"https://openalex.org/A5066190336","display_name":"Jonathan V Pelt","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I1308724467","display_name":"Florida Department of Agriculture and Consumer Services","ror":"https://ror.org/058nbms57","country_code":"US","type":"government","lineage":["https://openalex.org/I1308724467"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Jonathan V Pelt","raw_affiliation_strings":["Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","institution_ids":["https://openalex.org/I1308724467"]}]},{"author_position":"last","author":{"id":"https://openalex.org/A5056074841","display_name":"Ghislain Gerard","orcid":null,"observed_orcids":[]},"institutions":[{"id":"https://openalex.org/I1308724467","display_name":"Florida Department of Agriculture and Consumer Services","ror":"https://ror.org/058nbms57","country_code":"US","type":"government","lineage":["https://openalex.org/I1308724467"]}],"countries":["US"],"is_corresponding":false,"raw_author_name":"Ghislain Gerard","raw_affiliation_strings":["Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650"],"raw_orcid":null,"affiliations":[{"raw_affiliation_string":"Florida Department of Agriculture and Consumer Services, Bureau of Chemical Residue Laboratories, 3125 Connor Blvd, Building 3, Tallahassee, FL 32399-1650","institution_ids":["https://openalex.org/I1308724467"]}]}],"institutions":[],"countries_distinct_count":1,"institutions_distinct_count":1,"corresponding_author_ids":["https://openalex.org/A5075985200"],"corresponding_institution_ids":["https://openalex.org/I1308724467"],"apc_list":{"value":1868,"currency":"USD","value_usd":1868},"apc_paid":null,"fwci":2.1912,"has_fulltext":false,"cited_by_count":14,"citation_normalized_percentile":{"value":0.84872631,"is_in_top_1_percent":false,"is_in_top_10_percent":false},"cited_by_percentile_year":{"min":88,"max":97},"biblio":{"volume":"94","issue":"3","first_page":"931","last_page":"941"},"is_retracted":false,"is_paratext":false,"is_xpac":false,"primary_topic":{"id":"https://openalex.org/T11423","display_name":"Pesticide Residue Analysis and Safety","score":1.0,"subfield":{"id":"https://openalex.org/subfields/1106","display_name":"Food Science"},"field":{"id":"https://openalex.org/fields/11","display_name":"Agricultural and Biological Sciences"},"domain":{"id":"https://openalex.org/domains/1","display_name":"Life Sciences"}},"topics":[{"id":"https://openalex.org/T11423","display_name":"Pesticide Residue Analysis and Safety","score":1.0,"subfield":{"id":"https://openalex.org/subfields/1106","display_name":"Food Science"},"field":{"id":"https://openalex.org/fields/11","display_name":"Agricultural and Biological Sciences"},"domain":{"id":"https://openalex.org/domains/1","display_name":"Life Sciences"}},{"id":"https://openalex.org/T10180","display_name":"Analytical chemistry methods development","score":0.0,"subfield":{"id":"https://openalex.org/subfields/1602","display_name":"Analytical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}},{"id":"https://openalex.org/T10908","display_name":"Analytical Chemistry and Chromatography","score":0.0,"subfield":{"id":"https://openalex.org/subfields/1602","display_name":"Analytical Chemistry"},"field":{"id":"https://openalex.org/fields/16","display_name":"Chemistry"},"domain":{"id":"https://openalex.org/domains/3","display_name":"Physical Sciences"}}],"keywords":[{"id":"https://openalex.org/keywords/pesticide-residues","display_name":"pesticide residues","score":0.9959999918937683},{"id":"https://openalex.org/keywords/fresh-produce","display_name":"fresh produce","score":0.8159999847412109},{"id":"https://openalex.org/keywords/multiresidue-analysis","display_name":"multiresidue analysis","score":0.7919999957084656},{"id":"https://openalex.org/keywords/chlorothalonil","display_name":"chlorothalonil","score":0.8080000281333923},{"id":"https://openalex.org/keywords/tomato","display_name":"tomato","score":0.43799999356269836},{"id":"https://openalex.org/keywords/potato","display_name":"potato","score":0.9570000171661377},{"id":"https://openalex.org/keywords/cabbage","display_name":"cabbage","score":0.9750000238418579},{"id":"https://openalex.org/keywords/orange","display_name":"orange","score":0.6909999847412109},{"id":"https://openalex.org/keywords/green-beans","display_name":"green beans","score":0.8849999904632568}],"concepts":[{"id":"https://openalex.org/C43617362","wikidata":"https://www.wikidata.org/wiki/Q170050","display_name":"Chromatography","level":1,"score":0.792332649230957},{"id":"https://openalex.org/C162356407","wikidata":"https://www.wikidata.org/wiki/Q180809","display_name":"Mass spectrometry","level":2,"score":0.7424118518829346},{"id":"https://openalex.org/C185592680","wikidata":"https://www.wikidata.org/wiki/Q2329","display_name":"Chemistry","level":0,"score":0.702229380607605},{"id":"https://openalex.org/C172493649","wikidata":"https://www.wikidata.org/wiki/Q7843529","display_name":"Triple quadrupole mass spectrometer","level":5,"score":0.5946604609489441},{"id":"https://openalex.org/C123460561","wikidata":"https://www.wikidata.org/wiki/Q677065","display_name":"Gas chromatography","level":2,"score":0.5704932808876038},{"id":"https://openalex.org/C106289968","wikidata":"https://www.wikidata.org/wiki/Q202012","display_name":"Ion trap","level":3,"score":0.5693563222885132},{"id":"https://openalex.org/C27826464","wikidata":"https://www.wikidata.org/wiki/Q899060","display_name":"Quadrupole ion trap","level":4,"score":0.5584520697593689},{"id":"https://openalex.org/C205345274","wikidata":"https://www.wikidata.org/wiki/Q873009","display_name":"Gas chromatography\u2013mass spectrometry","level":3,"score":0.5277398824691772},{"id":"https://openalex.org/C39984356","wikidata":"https://www.wikidata.org/wiki/Q2121987","display_name":"Quadrupole","level":2,"score":0.5158923864364624},{"id":"https://openalex.org/C2777463227","wikidata":"https://www.wikidata.org/wiki/Q408047","display_name":"Acetonitrile","level":2,"score":0.5036048293113708},{"id":"https://openalex.org/C113196181","wikidata":"https://www.wikidata.org/wiki/Q485223","display_name":"Analytical Chemistry (journal)","level":2,"score":0.48793813586235046},{"id":"https://openalex.org/C4725764","wikidata":"https://www.wikidata.org/wiki/Q844704","display_name":"Extraction (chemistry)","level":2,"score":0.4405376613140106},{"id":"https://openalex.org/C71043704","wikidata":"https://www.wikidata.org/wiki/Q17144692","display_name":"Selected reaction monitoring","level":4,"score":0.2606305181980133},{"id":"https://openalex.org/C31827203","wikidata":"https://www.wikidata.org/wiki/Q874296","display_name":"Tandem mass spectrometry","level":3,"score":0.09206664562225342},{"id":"https://openalex.org/C184779094","wikidata":"https://www.wikidata.org/wiki/Q26383","display_name":"Atomic physics","level":1,"score":0.0},{"id":"https://openalex.org/C121332964","wikidata":"https://www.wikidata.org/wiki/Q413","display_name":"Physics","level":0,"score":0.0}],"mesh":[{"descriptor_ui":"D000097","descriptor_name":"Acetonitriles","qualifier_ui":"Q000737","qualifier_name":"chemistry","is_major_topic":true},{"descriptor_ui":"D002849","descriptor_name":"Chromatography, Gas","qualifier_ui":"Q000379","qualifier_name":"methods","is_major_topic":true},{"descriptor_ui":"D002853","descriptor_name":"Chromatography, Liquid","qualifier_ui":"Q000379","qualifier_name":"methods","is_major_topic":true},{"descriptor_ui":"D005504","descriptor_name":"Food Analysis","qualifier_ui":"Q000379","qualifier_name":"methods","is_major_topic":false},{"descriptor_ui":"D005506","descriptor_name":"Food Contamination","qualifier_ui":null,"qualifier_name":null,"is_major_topic":false},{"descriptor_ui":"D005638","descriptor_name":"Fruit","qualifier_ui":"Q000737","qualifier_name":"chemistry","is_major_topic":true},{"descriptor_ui":"D006219","descriptor_name":"Halogens","qualifier_ui":"Q000737","qualifier_name":"chemistry","is_major_topic":false},{"descriptor_ui":"D010573","descriptor_name":"Pesticide Residues","qualifier_ui":"Q000032","qualifier_name":"analysis","is_major_topic":true},{"descriptor_ui":"D010575","descriptor_name":"Pesticides","qualifier_ui":"Q000737","qualifier_name":"chemistry","is_major_topic":false},{"descriptor_ui":"D013058","descriptor_name":"Mass Spectrometry","qualifier_ui":"Q000379","qualifier_name":"methods","is_major_topic":true},{"descriptor_ui":"D014675","descriptor_name":"Vegetables","qualifier_ui":"Q000737","qualifier_name":"chemistry","is_major_topic":false}],"locations_count":2,"locations":[{"id":"doi:10.1093/jaoac/94.3.931","doi":"https://doi.org/10.1093/jaoac/94.3.931","is_oa":false,"landing_page_url":"https://doi.org/10.1093/jaoac/94.3.931","pdf_url":null,"source":{"id":"https://openalex.org/S103486911","display_name":"Journal of AOAC International","issn_l":"1060-3271","issn":["1060-3271","1944-7922"],"is_oa":false,"is_in_doaj":false,"is_core":true,"listed_in":["anvur-scientific","cwts-core","dongbi-b","jufo-1","medline","norway-1","poland-40","russia-white-list-2","vabb-shw"],"host_organization":"https://openalex.org/P4310311648","host_organization_name":"Oxford University Press","host_organization_lineage":["https://openalex.org/P4310311648","https://openalex.org/P4310311647"],"host_organization_lineage_names":["Oxford University Press","University of Oxford"],"type":"journal"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC INTERNATIONAL","raw_type":"journal-article"},{"id":"pmid:21797022","doi":null,"is_oa":false,"landing_page_url":"https://pubmed.ncbi.nlm.nih.gov/21797022","pdf_url":null,"source":{"id":"https://openalex.org/S4306525036","display_name":"PubMed","issn_l":null,"issn":null,"is_oa":false,"is_in_doaj":false,"is_core":false,"listed_in":[],"host_organization":"https://openalex.org/I1299303238","host_organization_name":"National Institutes of Health","host_organization_lineage":["https://openalex.org/I1299303238"],"host_organization_lineage_names":[],"type":"repository"},"license":null,"license_id":null,"version":"publishedVersion","is_accepted":true,"is_published":true,"raw_source_name":"Journal of AOAC International","raw_type":"Journal Article"}],"best_oa_location":null,"sustainable_development_goals":[{"display_name":"Zero hunger","score":0.800000011920929,"id":"https://metadata.un.org/sdg/2"},{"display_name":"Responsible consumption and production","score":0.5171999931335449,"id":"https://metadata.un.org/sdg/12"}],"study_designs":[],"awards":[],"funders":[],"has_content":{"pdf":false,"grobid_xml":false},"content_urls":null,"referenced_works_count":0,"referenced_works":[],"related_works":["https://openalex.org/W1920514480","https://openalex.org/W2318833464","https://openalex.org/W2163146170","https://openalex.org/W1588332043","https://openalex.org/W2463844884","https://openalex.org/W1563420471","https://openalex.org/W1964290729","https://openalex.org/W2296900455","https://openalex.org/W2380306029","https://openalex.org/W2002841932"],"abstract_inverted_index":{"A":[0],"rapid":[1],"and":[2,11,37,51,79,84,92,96,114,134,164,175,209],"inexpensive":[3],"multiresidue":[4],"method":[5,151],"for":[6,86,124],"determining":[7],"pesticides":[8,59],"in":[9,89,99,111,172,198,203,207,211],"fruits":[10],"vegetables":[12],"is":[13],"presented.":[14],"Extraction":[15],"of":[16,101,126,140,194,200],"a":[17,107,138,154,182,188],"15":[18,22],"g":[19,156],"sample":[20],"with":[21,29,41,48,119,187],"mL":[23,159],"acetonitrile":[24],"was":[25,54,117,131,143],"followed":[26],"by":[27,72,145],"buffering":[28],"magnesium":[30,52],"sulfate,":[31],"sodium":[32,34],"chloride,":[33],"citrate":[35],"dihydrate,":[36],"disodium":[38],"citrate.":[39],"Acidification":[40],"formic":[42],"acid":[43],"prior":[44,150],"to":[45,56,66,136,148],"dispersive":[46],"cleanup":[47],"aminopropyl":[49],"sorbent":[50],"sulfate":[53],"used":[55,153],"stabilize":[57],"base-sensitive":[58],"such":[60],"as":[61],"chlorothalonil.":[62],"Extracts":[63],"were":[64,70,94,170,196],"concentrated":[65],"2":[67],"g/mL.":[68],"Analyses":[69],"conducted":[71,171],"GC/ion":[73],"trap":[74],"detector":[75],"MS,":[76],"GC-halogen-specific":[77],"detector,":[78],"LC/triple":[80],"quadrupole":[81,185],"MS.":[82],"Accuracy":[83],"repeatability":[85],"166":[87],"compounds":[88,202],"tomato,":[90],"potato,":[91],"cabbage":[93],"70-120%":[95,195],"<20%":[97],"CV":[98],"85%":[100],"the":[102,127,149],"compounds,":[103],"respectively.":[104],"Reproducibility":[105],"over":[106],"4":[108,179],"month":[109],"period":[110],"multiple":[112,161],"commodities":[113],"analytical":[115],"conditions":[116],"62-124%,":[118],"CVs":[120],"better":[121],"than":[122],"30%":[123],"91%":[125],"compounds.":[128],"Supply":[129],"cost/sample":[130],"reduced":[132,144],"66%,":[133],"time":[135],"extract":[137],"batch":[139],"24":[141],"samples":[142],"half":[146],"compared":[147],"that":[152],"50":[155],"sample,":[157],"100":[158],"acetonitrile,":[160],"SPE":[162],"columns,":[163],"additional":[165],"instrumentation.":[166],"Additional":[167],"extraction":[168],"studies":[169],"tomatoes,":[173,208],"oranges,":[174],"green":[176,204],"beans":[177],"at":[178],"g/mL":[180],"using":[181],"GC/MS":[183],"triple":[184],"system":[186],"programmable":[189],"temperature":[190],"vaporization":[191],"inlet.":[192],"Recoveries":[193],"achieved":[197],"93%":[199],"all":[201],"beans,":[205],"95%":[206],"97%":[210],"oranges.":[212]},"counts_by_year":[{"year":2024,"cited_by_count":1},{"year":2022,"cited_by_count":1},{"year":2021,"cited_by_count":3},{"year":2018,"cited_by_count":1},{"year":2017,"cited_by_count":1},{"year":2015,"cited_by_count":1},{"year":2014,"cited_by_count":2},{"year":2013,"cited_by_count":3},{"year":2012,"cited_by_count":1}],"updated_date":"2026-10-31T12:09:11.096373","created_date":"2016-06-24T00:00:00"}
